C₁₂H₉FN₂O₃

Base Information

Chemical Name:C₁₂H₉FN₂O₃
CAS No.:1609264-25-6
Molecular Formula:C₁₂H₉FN₂O₃
Molecular Weight:248.213
Hs Code.:

C<sub>12</sub>H<sub>9</sub>FN<sub>2</sub>O<sub>3</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₂H₉FN₂O₃

Chemical Property:

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Technology Process of C₁₂H₉FN₂O₃

There total 3 articles about C₁₂H₉FN₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 35309-35-4,428518-31-4
5-oxopyrrolidine-3-carboxylic acid methyl ester

: 1609264-25-6
C₁₂H₉FN₂O₃

Guidance literature:: Multi-step reaction with 3 steps

1: caesium carbonate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / 1,4-dioxane / 16 h / 100 °C / Inert atmosphere

2: Column: lA / methanol; dichloromethane; carbon dioxide / Resolution of racemate; liquid CO₂

3: water; lithium hydroxide / methanol; tetrahydrofuran / 0.17 h / 20 °C

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; water; caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; lithium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; carbon dioxide;

Reference yield:

: 179898-34-1
3-bromo-5-fluorobenzonitrile

: 1609264-25-6
C₁₂H₉FN₂O₃

Guidance literature:: Multi-step reaction with 3 steps

1: caesium carbonate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / 1,4-dioxane / 16 h / 100 °C / Inert atmosphere

2: Column: lA / methanol; dichloromethane; carbon dioxide / Resolution of racemate; liquid CO₂

3: water; lithium hydroxide / methanol; tetrahydrofuran / 0.17 h / 20 °C

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; water; caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; lithium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; carbon dioxide;

Reference yield:

: 1609264-24-5
C₁₃H₁₁FN₂O₃

: 1609264-25-6
C₁₂H₉FN₂O₃

Guidance literature:: Multi-step reaction with 2 steps

1: Column: lA / methanol; dichloromethane; carbon dioxide / Resolution of racemate; liquid CO₂

2: water; lithium hydroxide / methanol; tetrahydrofuran / 0.17 h / 20 °C

With water; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane; carbon dioxide;