C₂₀H₁₆Cl₂N₆O₄S₂

Base Information

Chemical Name:C₂₀H₁₆Cl₂N₆O₄S₂
CAS No.:1422360-72-2
Molecular Formula:C₂₀H₁₆Cl₂N₆O₄S₂
Molecular Weight:539.423
Hs Code.:

C<sub>20</sub>H<sub>16</sub>Cl<sub>2</sub>N<sub>6</sub>O<sub>4</sub>S<sub>2</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₀H₁₆Cl₂N₆O₄S₂

Chemical Property:

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Technology Process of C₂₀H₁₆Cl₂N₆O₄S₂

There total 12 articles about C₂₀H₁₆Cl₂N₆O₄S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 12.0%

: 3144-09-0
methanesulfonamide

: 1203603-93-3
{[2-({[5-(2,6-dichlorophenyl)-1,2,4-triazin-3-yl]amino}methyl)-1,3-benzothiazol-5-yl]oxy}acetic acid

: 1422360-72-2
C₂₀H₁₆Cl₂N₆O₄S₂

Guidance literature:: With benzotriazol-1-ol; 1,8-diazabicyclo[5.4.0]undec-7-ene; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 16h; Inert atmosphere;
DOI:10.1021/jm301499r

Reference yield:

: 854059-90-8
5-methoxybenzothiazole-2-carboxaldehyde

: 1422360-72-2
C₂₀H₁₆Cl₂N₆O₄S₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium methylate; hydroxylamine hydrochloride / ethanol / 20 °C / Inert atmosphere

2.1: acetic acid; zinc / 3 h / 20 °C / Inert atmosphere

2.2: Inert atmosphere

3.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 50 - 85 °C / Inert atmosphere

4.1: boron tribromide / dichloromethane / 18 h / -78 - 20 °C / Inert atmosphere

5.1: potassium carbonate / acetone / 0.5 h / 20 °C / Inert atmosphere

5.2: 60 °C / Inert atmosphere

6.1: lithium hydroxide / tetrahydrofuran; water / 1.5 h / 20 °C / Inert atmosphere

7.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 16 h / 20 °C / Inert atmosphere

With hydroxylamine hydrochloride; sodium methylate; boron tribromide; potassium carbonate; benzotriazol-1-ol; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; lithium hydroxide; zinc; In tetrahydrofuran; ethanol; dichloromethane; water; acetone; acetonitrile;
DOI:10.1021/jm301499r

Reference yield:

: 1203605-11-1
5-methoxy-1,3-benzothiazole-2-carbaldehyde oxime

: 1422360-72-2
C₂₀H₁₆Cl₂N₆O₄S₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: acetic acid; zinc / 3 h / 20 °C / Inert atmosphere

1.2: Inert atmosphere

2.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 50 - 85 °C / Inert atmosphere

3.1: boron tribromide / dichloromethane / 18 h / -78 - 20 °C / Inert atmosphere

4.1: potassium carbonate / acetone / 0.5 h / 20 °C / Inert atmosphere

4.2: 60 °C / Inert atmosphere

5.1: lithium hydroxide / tetrahydrofuran; water / 1.5 h / 20 °C / Inert atmosphere

6.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 16 h / 20 °C / Inert atmosphere

With boron tribromide; potassium carbonate; benzotriazol-1-ol; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; lithium hydroxide; zinc; In tetrahydrofuran; dichloromethane; water; acetone; acetonitrile;
DOI:10.1021/jm301499r