Technology Process of C29H39Cl5N3O3P3
There total 3 articles about C29H39Cl5N3O3P3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: tetra-(n-butyl)ammonium iodide / butanone / 5 h / Reflux
2: potassium hydroxide / methanol / 10 h / Reflux
3: 2,2,4,4,6,6-hexachloro-1,3,5-triaza-2,4,6-triphosphorine; potassium carbonate / acetone / 1 h / Reflux
With
2,2,4,4,6,6-hexachloro-1,3,5-triaza-2,4,6-triphosphorine; tetra-(n-butyl)ammonium iodide; potassium carbonate; potassium hydroxide;
In
methanol; acetone; butanone;
2: Claisen Schmidt condensation;
DOI:10.1139/V10-057
- Guidance literature:
-
Multi-step reaction with 3 steps
1: tetra-(n-butyl)ammonium iodide / butanone / 5 h / Reflux
2: potassium hydroxide / methanol / 10 h / Reflux
3: 2,2,4,4,6,6-hexachloro-1,3,5-triaza-2,4,6-triphosphorine; potassium carbonate / acetone / 1 h / Reflux
With
2,2,4,4,6,6-hexachloro-1,3,5-triaza-2,4,6-triphosphorine; tetra-(n-butyl)ammonium iodide; potassium carbonate; potassium hydroxide;
In
methanol; acetone; butanone;
2: Claisen Schmidt condensation;
DOI:10.1139/V10-057
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium hydroxide / methanol / 10 h / Reflux
2: 2,2,4,4,6,6-hexachloro-1,3,5-triaza-2,4,6-triphosphorine; potassium carbonate / acetone / 1 h / Reflux
With
2,2,4,4,6,6-hexachloro-1,3,5-triaza-2,4,6-triphosphorine; potassium carbonate; potassium hydroxide;
In
methanol; acetone;
1: Claisen Schmidt condensation;
DOI:10.1139/V10-057
