Pt((C₆H₅)2PCH₂CH₂P(C₆H₅)2)(SCH(CH₂CH₂)2NCH₃)2

Base Information

Chemical Name:Pt((C₆H₅)2PCH₂CH₂P(C₆H₅)2)(SCH(CH₂CH₂)2NCH₃)2
CAS No.:146084-47-1
Molecular Formula:C₃₈H₄₈N₂P₂PtS₂
Molecular Weight:853.972
Hs Code.:

Pt((C<sub>6</sub>H<sub>5</sub>)2PCH<sub>2</sub>CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)(SCH(CH<sub>2</sub>CH<sub>2</sub>)2NCH<sub>3</sub>)2

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Chemical Property of Pt((C₆H₅)2PCH₂CH₂P(C₆H₅)2)(SCH(CH₂CH₂)2NCH₃)2

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Technology Process of Pt((C₆H₅)2PCH₂CH₂P(C₆H₅)2)(SCH(CH₂CH₂)2NCH₃)2

There total 1 articles about Pt((C₆H₅)2PCH₂CH₂P(C₆H₅)2)(SCH(CH₂CH₂)2NCH₃)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 83095-83-4,14647-25-7
[platinum(II)dichloride(1,2-bis(diphenylphosphino)ethane)]

: 153851-37-7
4-mercato-1-methylpiperidine, sodium salt

: 146084-47-1
Pt((C₆H₅)2PCH₂CH₂P(C₆H₅)2)(SCH(CH₂CH₂)2NCH₃)2

Guidance literature:: In methanol; acetonitrile; byproducts: NaCl; react. under N2, slow addn. of NaC5H9N(CH3)SH in MeOH to a suspension of PtCl2(dppe) in acetonitrile, stirring for 48 h; evapg. under vac., keeping under N2 for 1 d, several extns. with acetonitrile, concg. the solns., crystn., elem. anal.;
DOI:10.1039/DT9920002817

Reference yield: 79.5%

: 83095-83-4,14647-25-7
[platinum(II)dichloride(1,2-bis(diphenylphosphino)ethane)]

: 146084-47-1
Pt((C₆H₅)2PCH₂CH₂P(C₆H₅)2)(SCH(CH₂CH₂)2NCH₃)2

: 143-66-8
sodium tetraphenyl borate

: {(Pt(SC₅H₉N(CH₃))((C₆H₅)2PCH₂CH₂P(C₆H₅)2))2}⁽²⁺⁾*2B(C₆H₅)4^(1-)={(Pt(SC₅H₉N(CH₃))((C₆H₅)2PC₂H₄P(C₆H₅)2))2}{B(C₆H₅)4}2

Guidance literature:: With KPF₆; In dichloromethane; acetonitrile; byproducts: KCl; react. under N2, addn. of Pt(SC5H9NMe)2(dppe) in acetonitrile to a suspension of PtCl2(dppe) in CH2Cl2, addn. of KPF6 in acetonitrile when getting a clear soln., pptn. of KCl, stirring for some minutes; evapg. in vac., addn. of acetonitrile, filtration, addn. of NaBPh4 in acetonitrile, stirring for some minutes, crystn., filtration, washing with MeOH, further crystals by slow evapn. of the mother-liquor under a very slow stream of N2, elem. anal.;
DOI:10.1039/DT9920002817

Reference yield: 51.6%

: (trimethylplatinum(IV) iodide)4

: 146084-47-1
Pt((C₆H₅)2PCH₂CH₂P(C₆H₅)2)(SCH(CH₂CH₂)2NCH₃)2

: [(dppe)Pt(μ-SCH(CH2CH2)2NMe)2PtIMe3]

Guidance literature:: In benzene; inert atmosphere; stirring for 2.5 d; collection (filtration), washing (C6H6), drying (vac.); elem. anal.;
DOI:10.1016/s0020-1693(97)05674-0