Cl₂PP(C₆H₅)2W(CO)5

Base Information

Chemical Name:Cl₂PP(C₆H₅)2W(CO)5
CAS No.:147074-68-8
Molecular Formula:C₁₇H₁₀Cl₂O₅P₂W
Molecular Weight:610.967
Hs Code.:

Cl<sub>2</sub>PP(C<sub>6</sub>H<sub>5</sub>)2W(CO)5

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Cl₂PP(C₆H₅)2W(CO)5

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Technology Process of Cl₂PP(C₆H₅)2W(CO)5

There total 1 articles about Cl₂PP(C₆H₅)2W(CO)5 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.9%

: 18399-62-7
W(CO)5(PPh2H)

: 7719-12-2,52843-90-0
phosphorus trichloride

: 147074-68-8
Cl₂PP(C₆H₅)2W(CO)5

Guidance literature:: With triethylamine; In tetrahydrofuran; byproducts: (HNEt3)Cl; dissolution of phosphane and PCl3 in THF at room temp. (under exclusion of air and moisture, under Ar), addn. of NEt3, pptn. of (HNEt3)Cl, stirring for 3 h at room temp. and for 1 h at 50°C; reducing solvent in volume to a half under vacuum, filtn., evapn. of filtrate to dryness at 40-50°C, recrystn. from CH2Cl2/n-pentane, elem. anal.;

Reference yield: 63.6%

: 18399-62-7
W(CO)5(PPh2H)

: 147074-68-8
Cl₂PP(C₆H₅)2W(CO)5

: 147074-69-9
1,3-bis(pentacarbonyltungsten⁽⁰⁾)-1,1',3,3'-tetraphenyl-2-chlorotriphosphane

Guidance literature:: With triethylamine; In tetrahydrofuran; byproducts: (HNEt3)Cl; dissolution of phosphane and PCl3 in THF (under exclusion of air and moisture, under Ar), addn. of NEt3, stirring for 6 h, pptn. of (HNEt3)Cl, warming to 40°C for 30 min; filtn., evapn. of solvent in vacuo, addn. of n-pentane, pptn., recrystn. from CH2Cl2/n-pentane, elem. anal.;