ruthenocenyl dicyclohexylphosphane

Base Information

Chemical Name:ruthenocenyl dicyclohexylphosphane
CAS No.:1356191-94-0
Molecular Formula:C₂₂H₃₁PRu
Molecular Weight:427.532
Hs Code.:

Synonyms:

Suppliers and Price of ruthenocenyl dicyclohexylphosphane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ruthenocenyl dicyclohexylphosphane

Chemical Property:

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Technology Process of ruthenocenyl dicyclohexylphosphane

There total 1 articles about ruthenocenyl dicyclohexylphosphane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 70210-62-7
monoiodoruthenocene

: 16523-54-9
chlorodicyclohexylphosphane

: 1356191-94-0
ruthenocenyl dicyclohexylphosphane

Guidance literature:: With n-butyllithium; In tetrahydrofuran; under Ar or N2, Schlenk technique; soln. of n-BuLi added dropwise to soln. of Ru compd. at -60°C, mixt. stirred at room temp. for 0.5 h, cooled to -30°C, P compd. added dropwise, mixt. stirred at room temp. for 1 h; concn. under vac., chromy. (Alox, n-hexane/Et2O 5/1), dried under vac.; contaminated;
DOI:10.1002/ejic.201100842

Reference yield:

: 7782-49-2
selenium

: 1356191-94-0
ruthenocenyl dicyclohexylphosphane

: 1356192-00-1
ruthenocenyl dicyclohexylselenophosphane

Guidance literature:: In toluene; Se (1.2 equiv.) added to soln. of Ru complex in toluene, mixt. stirred at 100°C for 1 h, cooled to room temp.; soln. filtered through Celite, filtrate dried under vac.;
DOI:10.1002/ejic.201100842