C₂₇H₃₂N₂O₅S

Base Information

Chemical Name:C₂₇H₃₂N₂O₅S
CAS No.:1360744-14-4
Molecular Formula:C₂₇H₃₂N₂O₅S
Molecular Weight:496.627
Hs Code.:

C<sub>27</sub>H<sub>32</sub>N<sub>2</sub>O<sub>5</sub>S

Synonyms:

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Chemical Property of C₂₇H₃₂N₂O₅S

Chemical Property:

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Technology Process of C₂₇H₃₂N₂O₅S

There total 13 articles about C₂₇H₃₂N₂O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1360744-13-3
C₂₉H₃₆N₂O₅S

: 1360744-14-4
C₂₇H₃₂N₂O₅S

Guidance literature:: With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In dichloromethane; at -78 ℃; Reflux;
DOI:10.1002/chem.201102101

Reference yield:

: 1360744-10-0
C₇H₉IO₂

: 1360744-14-4
C₂₇H₃₂N₂O₅S

Guidance literature:: Multi-step reaction with 12 steps

1.1: 1H-imidazole; dmap / dichloromethane / 24 h / 20 °C

2.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / N,N-dimethyl-formamide / 24 h / -78 - 20 °C

3.1: platinum(II) chloride / toluene / 1.45 h / 80 °C

4.1: dimethylsulfide borane complex / tetrahydrofuran / 0 - 20 °C

4.2: 1 h / 0 - 20 °C

5.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 20 °C

5.2: 3 h / 20 °C

6.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / Reflux

7.1: diisobutylaluminium hydride / dichloromethane; toluene / 0.5 h / -78 °C

8.1: potassium tert-butylate / tetrahydrofuran / 1 h / 0 °C

9.1: zinc dibromide / dichloromethane / 2 h / Inert atmosphere; Reflux

10.1: triethylamine / dichloromethane / 10 h

11.1: tetrabutyl ammonium fluoride / tetrahydrofuran

12.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / -78 °C / Reflux

With 1H-imidazole; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; dmap; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; 2,2'-azobis(isobutyronitrile); dimethylsulfide borane complex; potassium tert-butylate; tetrabutyl ammonium fluoride; tri-n-butyl-tin hydride; sodium hydride; diisobutylaluminium hydride; triethylamine; platinum(II) chloride; zinc dibromide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene; mineral oil; 2.1: Sonogashira coupling / 4.1: Hydroboration reaction / 6.1: Barton-McCombie deoxygenation / 8.1: Wittig reaction;
DOI:10.1002/chem.201102101

Reference yield:

: C₁₅H₂₂N₂O₄

: 1360744-14-4
C₂₇H₃₂N₂O₅S

Guidance literature:: Multi-step reaction with 12 steps

1.1: triethylamine / dichloromethane / 1 h

2.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / N,N-dimethyl-formamide / 24 h / -78 - 20 °C

3.1: platinum(II) chloride / toluene / 1.45 h / 80 °C

4.1: dimethylsulfide borane complex / tetrahydrofuran / 0 - 20 °C

4.2: 1 h / 0 - 20 °C

5.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 20 °C

5.2: 3 h / 20 °C

6.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / Reflux

7.1: diisobutylaluminium hydride / dichloromethane; toluene / 0.5 h / -78 °C

8.1: potassium tert-butylate / tetrahydrofuran / 1 h / 0 °C

9.1: zinc dibromide / dichloromethane / 2 h / Inert atmosphere; Reflux

10.1: triethylamine / dichloromethane / 10 h

11.1: tetrabutyl ammonium fluoride / tetrahydrofuran

12.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / -78 °C / Reflux

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; 2,2'-azobis(isobutyronitrile); dimethylsulfide borane complex; potassium tert-butylate; tetrabutyl ammonium fluoride; tri-n-butyl-tin hydride; sodium hydride; diisobutylaluminium hydride; triethylamine; platinum(II) chloride; zinc dibromide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene; mineral oil; 2.1: Sonogashira coupling / 4.1: Hydroboration reaction / 6.1: Barton-McCombie deoxygenation / 8.1: Wittig reaction;
DOI:10.1002/chem.201102101