Technology Process of C66H86N14O12
There total 3 articles about C66H86N14O12 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
copper(ll) sulfate pentahydrate; sodium L-ascorbate;
In
water; dimethyl sulfoxide;
DOI:10.1016/j.bmcl.2012.04.040
- Guidance literature:
-
Multi-step reaction with 3 steps
1: hydrogenchloride; palladium 10% on activated carbon / methanol; water / 760.05 Torr / Inert atmosphere
2: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 4 h / 20 °C
3: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; dimethyl sulfoxide
With
hydrogenchloride; copper(ll) sulfate pentahydrate; palladium 10% on activated carbon; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; sodium L-ascorbate; N-ethyl-N,N-diisopropylamine;
In
methanol; water; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.04.040
- Guidance literature:
-
Multi-step reaction with 2 steps
1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 4 h / 20 °C
2: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; dimethyl sulfoxide
With
copper(ll) sulfate pentahydrate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; sodium L-ascorbate; N-ethyl-N,N-diisopropylamine;
In
water; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.04.040