{bis(benzyl-tert-butylamino)boron}tetrabromo borate

Base Information

Chemical Name:{bis(benzyl-tert-butylamino)boron}tetrabromo borate
CAS No.:106542-71-6
Molecular Formula:BBr₄*C₂₂H₃₂BN₂
Molecular Weight:665.747
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of {bis(benzyl-tert-butylamino)boron}tetrabromo borate

Chemical Property:

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Technology Process of {bis(benzyl-tert-butylamino)boron}tetrabromo borate

There total 2 articles about {bis(benzyl-tert-butylamino)boron}tetrabromo borate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 106367-62-8
bis(benzyl-tert-butylamino)boron fluoride

: 10294-33-4
boron tribromide

: 106542-71-6
{bis(benzyl-tert-butylamino)boron}tetrabromo borate

Guidance literature:: In dichloromethane; react. in dry N2 or in vac. with exclosure of moisture; BBr3 was added to a soln. of the B-compound in CH2Cl2 with stirring at -50°C; the soln. was allowed to warm to 0°C; it was stirred for 15 min at this temp.;; evapd. in vac., volatiles condensed at -196°C; product remains as the residue; elem. anal.;;

Reference yield:

: lithium-benzyl-tert-butylamide

: 106542-71-6
{bis(benzyl-tert-butylamino)boron}tetrabromo borate

Guidance literature:: Multi-step reaction with 2 steps

1: hexane

2: dichloromethane

In hexane; dichloromethane;

Reference yield:

: 106542-71-6
{bis(benzyl-tert-butylamino)boron}tetrabromo borate

: lithium-benzyl-tert-butylamide

: 91573-50-1
bis(benzyl-tert-butylamino)borane

Guidance literature:: In hexane; react. in dry N2 or in vac. with exclosure of moisture; to a suspension of B-compound in hexane a soln. of lithium-benzyl-tert-butylamide was added dropwise at room temp. within 1 h; stirred for 24 h at room temp.;; filtration; (11)B NMR;