[RuClCp(PPh3)-μ-3,7-dimethyl-1,3,7-triaza-5-phosphabicyclo[3.3.1]nonane-1κP:2κ2N,N'-Co(acetylacetonato-κ2O,O')2]*H2O

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Chemical Name:[RuClCp(PPh3)-μ-3,7-dimethyl-1,3,7-triaza-5-phosphabicyclo[3.3.1]nonane-1κP:2κ2N,N'-Co(acetylacetonato-κ2O,O')2]*H2O
CAS No.:1019207-44-3
Molecular Formula:C₄₀H₅₀ClCoN₃O₄P₂Ru*H₂O
Molecular Weight:912.334
Hs Code.:

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Chemical Property of [RuClCp(PPh3)-μ-3,7-dimethyl-1,3,7-triaza-5-phosphabicyclo[3.3.1]nonane-1κP:2κ2N,N'-Co(acetylacetonato-κ2O,O')2]*H2O

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Technology Process of [RuClCp(PPh3)-μ-3,7-dimethyl-1,3,7-triaza-5-phosphabicyclo[3.3.1]nonane-1κP:2κ2N,N'-Co(acetylacetonato-κ2O,O')2]*H2O

There total 2 articles about [RuClCp(PPh3)-μ-3,7-dimethyl-1,3,7-triaza-5-phosphabicyclo[3.3.1]nonane-1κP:2κ2N,N'-Co(acetylacetonato-κ2O,O')2]*H2O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 946088-18-2
[RuClCp(3,7-dimethyl-1,3,7-triaza-5-phosphabicyclo[3.3.1]nonane)(PPh₃)]*(OSO₂CF₃)

: cobalt acetylacetonate

: 1019207-44-3
[RuClCp(PPh3)-μ-3,7-dimethyl-1,3,7-triaza-5-phosphabicyclo[3.3.1]nonane-1κP:2κ2N,N'-Co(acetylacetonato-κ2O,O')2]*H2O

Guidance literature:: In methanol; byproducts: CF3SO3H; (Ar); Co complex added to a soln. of Ru complex, stirred for 20 min, refluxed for 4 h; concd. at room temp., pptd. with aq. soln. of KCl, stirred for 10 min, sonicated with ultrasound, filtered, washed (KCl soln., cold H2O, cold isopropanol), dried (vac.), recrystd. (MeOH/EtOH);
DOI:10.1039/c0dt00571a

Reference yield: 55.0%

: 946088-18-2
[RuClCp(3,7-dimethyl-1,3,7-triaza-5-phosphabicyclo[3.3.1]nonane)(PPh₃)]*(OSO₂CF₃)

: 7732-18-5
water

: cobalt(II) aceylacetonate

: 1019207-44-3
[RuClCp(PPh3)-μ-3,7-dimethyl-1,3,7-triaza-5-phosphabicyclo[3.3.1]nonane-1κP:2κ2N,N'-Co(acetylacetonato-κ2O,O')2]*H2O

Guidance literature:: In methanol; addn. of cobalt compd. to methanolic soln. of cobalt compd., stirring atroom temp. for dissolving compds., refluxing for 3.5 h; concg., addn. of pentane, filtration, washing with water, recrystn. (ethanol), elem. anal.;
DOI:10.1021/ic702239w