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Technology Process of C18H24N2O6

C18H24N2O6

Base Information Edit
C<sub>18</sub>H<sub>24</sub>N<sub>2</sub>O<sub>6</sub>

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The product has achieved commercial mass production*data from LookChem market partment
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Chemical Property of C18H24N2O6 Edit
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Technology Process of C18H24N2O6

There total 1 articles about C18H24N2O6 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(R)-4-hydroxy-1-undecene
122606-77-3

(R)-4-hydroxy-1-undecene

3,5-dinitrobenoyl chloride
99-33-2

3,5-dinitrobenoyl chloride

C<sub>18</sub>H<sub>24</sub>N<sub>2</sub>O<sub>6</sub>
1263532-28-0

C18H24N2O6

Guidance literature:
With pyridine; In dichloromethane; at 20 ℃; for 3.5h; optical yield given as %ee; Inert atmosphere;
DOI:10.1002/anie.201004746

Reference yield:

C<sub>18</sub>H<sub>24</sub>N<sub>2</sub>O<sub>6</sub>
1263532-28-0

C18H24N2O6

C<sub>34</sub>H<sub>48</sub>O<sub>4</sub>Si

C34H48O4Si

Guidance literature:
Multi-step reaction with 2 steps
1: sodium methylate / methanol / 2 h / 20 °C / Inert atmosphere
2: dmap / dichloromethane / 21 h / Inert atmosphere
With dmap; sodium methylate; In methanol; dichloromethane;
DOI:10.1002/anie.201004746

Reference yield:

C<sub>18</sub>H<sub>24</sub>N<sub>2</sub>O<sub>6</sub>
1263532-28-0

C18H24N2O6

C<sub>32</sub>H<sub>44</sub>O<sub>4</sub>Si

C32H44O4Si

Guidance literature:
Multi-step reaction with 3 steps
1: sodium methylate / methanol / 2 h / 20 °C / Inert atmosphere
2: dmap / dichloromethane / 21 h / Inert atmosphere
3: Hoveyda-Grubbs catalyst second generation; p-benzoquinone / 5,5-dimethyl-1,3-cyclohexadiene / 24 h / Inert atmosphere; Reflux
With dmap; Hoveyda-Grubbs catalyst second generation; sodium methylate; p-benzoquinone; In methanol; 5,5-dimethyl-1,3-cyclohexadiene; dichloromethane;
DOI:10.1002/anie.201004746
upstream raw materials:

(R)-4-hydroxy-1-undecene

3,5-dinitrobenoyl chloride

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