Technology Process of C41H45NO6SSi
There total 3 articles about C41H45NO6SSi which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: tri-tert-butyl phosphine; potassium tert-butylate; bis(dibenzylideneacetone)-palladium(0) / toluene / 80 °C
2: Iodine monochloride / dichloromethane; acetonitrile / 25 °C
3: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / water; toluene / Reflux
4: Iodine monochloride / dichloromethane; acetonitrile / 25 °C
5: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / water; toluene / Reflux
With
tetrakis(triphenylphosphine) palladium(0); tri-tert-butyl phosphine; potassium tert-butylate; Iodine monochloride; sodium carbonate; bis(dibenzylideneacetone)-palladium(0);
In
dichloromethane; water; toluene; acetonitrile;
3: Suzuki coupling / 5: Suzuki coupling;
DOI:10.1021/ic201446x
- Guidance literature:
-
Multi-step reaction with 2 steps
1: Iodine monochloride / dichloromethane; acetonitrile / 25 °C
2: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / water; toluene / Reflux
With
tetrakis(triphenylphosphine) palladium(0); Iodine monochloride; sodium carbonate;
In
dichloromethane; water; toluene; acetonitrile;
2: Suzuki coupling;
DOI:10.1021/ic201446x
- Guidance literature:
-
With
tetrakis(triphenylphosphine) palladium(0); sodium carbonate;
In
water; toluene;
Reflux;
DOI:10.1021/ic201446x