C₃₈H₅₀N₄O₁₀

Base Information

• Chemical Name: C₃₈H₅₀N₄O₁₀
• CAS No.: 1426832-93-0
• Molecular Formula: C₃₈H₅₀N₄O₁₀
• Molecular Weight: 722.836
• Mol file: 1426832-93-0.mol

Synonyms:

Chemical Property of C₃₈H₅₀N₄O₁₀

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₈H₅₀N₄O₁₀

There total 8 articles about C₃₈H₅₀N₄O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C53H60N4O12 (1426832-91-8) → C38H50N4O10 (1426832-93-0)

Guidance literature:

With piperidine; In N,N-dimethyl-formamide; at 20 ℃;

DOI:10.1002/chem.201202998

Reference yield:

3-methoxy-N-methylaniline (14318-66-2) → C38H50N4O10 (1426832-93-0)

Guidance literature:

Multi-step reaction with 7 steps

1.1: potassium carbonate / acetone / 14 h / Reflux

2.1: trichlorophosphate / 0.5 h / 0 °C

2.2: 0.5 h / 0 - 20 °C

3.1: boron tribromide / dichloromethane / 2.5 h / -78 - 20 °C

4.1: piperidine / tetrahydrofuran / 6 h / Reflux; Inert atmosphere

5.1: lithium hydroxide; methanol / water / 2 h / Reflux

6.1: dicyclohexyl-carbodiimide; benzotriazol-1-ol; dmap / dichloromethane / 14 h / 20 °C

7.1: piperidine / N,N-dimethyl-formamide / 20 °C

With piperidine; methanol; dmap; boron tribromide; potassium carbonate; benzotriazol-1-ol; dicyclohexyl-carbodiimide; lithium hydroxide; trichlorophosphate; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; acetone;

DOI:10.1002/chem.201202998

Reference yield:

methyl N-(3-methoxyphenyl)-N-methylglycinate (1249992-01-5) → C38H50N4O10 (1426832-93-0)

Guidance literature:

Multi-step reaction with 6 steps

1.1: trichlorophosphate / 0.5 h / 0 °C

1.2: 0.5 h / 0 - 20 °C

2.1: boron tribromide / dichloromethane / 2.5 h / -78 - 20 °C

3.1: piperidine / tetrahydrofuran / 6 h / Reflux; Inert atmosphere

4.1: lithium hydroxide; methanol / water / 2 h / Reflux

5.1: dicyclohexyl-carbodiimide; benzotriazol-1-ol; dmap / dichloromethane / 14 h / 20 °C

6.1: piperidine / N,N-dimethyl-formamide / 20 °C

With piperidine; methanol; dmap; boron tribromide; benzotriazol-1-ol; dicyclohexyl-carbodiimide; lithium hydroxide; trichlorophosphate; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;

DOI:10.1002/chem.201202998

upstream raw materials:

m-Anisidine

3-methoxy-N-methylaniline

methyl N-(3-methoxyphenyl)-N-methylglycinate

C₁₂H₁₅NO₄

Downstream raw materials:

C₈₈H₁₀₄N₈O₂₁