(2E,4E)-4-[(4-bromophenoxy)imino]-2-butenoic acid 2,3,4,5,6-pentafluorophenyl ester

Base Information

Chemical Name:(2E,4E)-4-[(4-bromophenoxy)imino]-2-butenoic acid 2,3,4,5,6-pentafluorophenyl ester
CAS No.:1627150-06-4
Molecular Formula:C₁₆H₇BrF₅NO₃
Molecular Weight:436.132
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2E,4E)-4-[(4-bromophenoxy)imino]-2-butenoic acid 2,3,4,5,6-pentafluorophenyl ester

Chemical Property:

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Technology Process of (2E,4E)-4-[(4-bromophenoxy)imino]-2-butenoic acid 2,3,4,5,6-pentafluorophenyl ester

There total 3 articles about (2E,4E)-4-[(4-bromophenoxy)imino]-2-butenoic acid 2,3,4,5,6-pentafluorophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 771-61-9
2,3,4,5,6-pentafluorophenol

: C₁₀H₈BrNO₃

: 1627150-06-4
(2E,4E)-4-[(4-bromophenoxy)imino]-2-butenoic acid 2,3,4,5,6-pentafluorophenyl ester

Guidance literature:: With dmap; ethylene dichloride hydrochloride; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1002/chem.201402217

Reference yield:

: 1007570-12-8
O-(4-bromophenyl)hydroxylamine hydrochloride

: 1627150-06-4
(2E,4E)-4-[(4-bromophenoxy)imino]-2-butenoic acid 2,3,4,5,6-pentafluorophenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 0.5 h / 20 °C / Inert atmosphere

2: lithium hydroxide / tetrahydrofuran; water / 0.5 h / 20 °C

3: ethylene dichloride hydrochloride; dmap / dichloromethane / 2 h / 20 °C

With pyridine; dmap; ethylene dichloride hydrochloride; lithium hydroxide; In tetrahydrofuran; dichloromethane; water;
DOI:10.1002/chem.201402217

Reference yield:

: 1627150-22-4
C₁₂H₁₂BrNO₃

: 1627150-06-4
(2E,4E)-4-[(4-bromophenoxy)imino]-2-butenoic acid 2,3,4,5,6-pentafluorophenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: lithium hydroxide / tetrahydrofuran; water / 0.5 h / 20 °C

2: ethylene dichloride hydrochloride; dmap / dichloromethane / 2 h / 20 °C

With dmap; ethylene dichloride hydrochloride; lithium hydroxide; In tetrahydrofuran; dichloromethane; water;
DOI:10.1002/chem.201402217