ZnC₂₀N₄H₂(CH₃)4(C₆H₁₃)4C₆H₃(C₄H₉)2C₆H₄C₂PO(OC₂H₅)2

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Chemical Name:ZnC₂₀N₄H₂(CH₃)4(C₆H₁₃)4C₆H₃(C₄H₉)2C₆H₄C₂PO(OC₂H₅)2
CAS No.:767352-15-8
Molecular Formula:C₇₄H₁₀₁N₄O₃PZn
Molecular Weight:1191
Hs Code.:

ZnC<sub>20</sub>N<sub>4</sub>H<sub>2</sub>(CH<sub>3</sub>)4(C<sub>6</sub>H<sub>13</sub>)4C<sub>6</sub>H<sub>3</sub>(C<sub>4</sub>H<sub>9</sub>)2C<sub>6</sub>H<sub>4</sub>C<sub>2</sub>PO(OC<sub>2</sub>H<sub>5</sub>)2

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Chemical Property of ZnC₂₀N₄H₂(CH₃)4(C₆H₁₃)4C₆H₃(C₄H₉)2C₆H₄C₂PO(OC₂H₅)2

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Technology Process of ZnC₂₀N₄H₂(CH₃)4(C₆H₁₃)4C₆H₃(C₄H₉)2C₆H₄C₂PO(OC₂H₅)2

There total 1 articles about ZnC₂₀N₄H₂(CH₃)4(C₆H₁₃)4C₆H₃(C₄H₉)2C₆H₄C₂PO(OC₂H₅)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 288613-51-4
ZnC₂₀N₄H₂(CH₃)4(C₆H₁₃)4C₆H₃(C₄H₉)2C₆H₄C₂H

: 814-49-3
diethyl chlorophosphate

: 767352-15-8
ZnC₂₀N₄H₂(CH₃)4(C₆H₁₃)4C₆H₃(C₄H₉)2C₆H₄C₂PO(OC₂H₅)2

Guidance literature:: With cadmium(II) chloride; In tetrahydrofuran; inert atm.; to a THF-soln. of Zn-porphyrin LiHMDA was added at -78°C, stirred for 15 min, CdCl2 was added, stirred for 30 min, phosphonate in THF was added, stirred at -78°C for 1.5 h, warmed to room temp., stirred for 30 min; poured to CH2Cl2, neutralised with satd. aq. Na2CO3, washed with H2O, dried over MgSO4, evapd., mixed with Zn(CH3CO2)2 in CH2Cl2-CH3OH, heated for 5 min, evapd. to dryness,extd. with CH2Cl2, filtered, column chromy. (silica, CH2Cl2-CH3OH);
DOI:10.1039/b402083a

Reference yield: 30.0%

: 767352-15-8
ZnC₂₀N₄H₂(CH₃)4(C₆H₁₃)4C₆H₃(C₄H₉)2C₆H₄C₂PO(OC₂H₅)2

: ZnC₂₀N₄H₂(CH₃)4(C₆H₁₃)4C₆H₃(C₄H₉)2C₆H₄C₂H₂PH₂

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; inert atm.; a soln. of complex in diethyl ether was added LiAlH4 at 0°C, stirred at 0°C for 2 h; transferred to CH2Cl2, brine was added, the mixt. was stirred for 10 min, the organic phase was sepd., concd. in vac., dissolved in THF, chromd.on silica gel column (THF);
DOI:10.1039/b402083a