Technology Process of C24H42
There total 4 articles about C24H42 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: aluminum (III) chloride / 3.5 h / Cooling with ice; Reflux
2.1: magnesium / diethyl ether / Reflux; Inert atmosphere
2.2: 2 h / Reflux; Inert atmosphere
2.3: Inert atmosphere
3.1: 5%-palladium/activated carbon; perchloric acid; hydrogen; acetic acid / 7500.75 Torr
With
aluminum (III) chloride; perchloric acid; 5%-palladium/activated carbon; hydrogen; magnesium; acetic acid;
In
diethyl ether;
1.1: Friedel-Crafts reaction / 2.2: Grignard reaction / 2.3: Grignard reaction;
DOI:10.1007/s11743-009-1165-z
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: magnesium / diethyl ether / Reflux; Inert atmosphere
1.2: 2 h / Reflux; Inert atmosphere
1.3: Inert atmosphere
2.1: 5%-palladium/activated carbon; perchloric acid; hydrogen; acetic acid / 7500.75 Torr
With
perchloric acid; 5%-palladium/activated carbon; hydrogen; magnesium; acetic acid;
In
diethyl ether;
1.2: Grignard reaction / 1.3: Grignard reaction;
DOI:10.1007/s11743-009-1165-z
- Guidance literature:
-
With
perchloric acid; 5%-palladium/activated carbon; hydrogen; acetic acid;
under 7500.75 Torr;
DOI:10.1007/s11743-009-1165-z
