4-(4-methylbenzoselenoyl)morpholine

Base Information

Chemical Name:4-(4-methylbenzoselenoyl)morpholine
CAS No.:139546-54-6
Molecular Formula:C12H15NOSe
Molecular Weight:268.21400
Hs Code.:
Mol file:139546-54-6.mol

Synonyms:Morpholin-4-yl-p-tolyl-methaneselone;

Suppliers and Price of 4-(4-methylbenzoselenoyl)morpholine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 4-(4-methylbenzoselenoyl)morpholine

Chemical Property:

PSA：12.47000
LogP:1.02410

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4-(4-methylbenzoselenoyl)morpholine

There total 3 articles about 4-(4-methylbenzoselenoyl)morpholine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 162274-51-3
4-<(Diphenylphosphinoyl)(p-tolyl)methyl>morpholine

: 139546-54-6
4-(4-Methylselenobenzoyl)morpholine

Guidance literature:: With selenium; n-butyllithium; In tetrahydrofuran; hexane; for 1h; Ambient temperature;

Reference yield:

: 104-87-0
4-methyl-benzaldehyde

: 139546-54-6
4-(4-Methylselenobenzoyl)morpholine

Guidance literature:: Multi-step reaction with 2 steps

2: 75 percent / BuLi, Se / tetrahydrofuran; hexane / 1 h / Ambient temperature

With selenium; n-butyllithium; In tetrahydrofuran; hexane;

Reference yield:

: 110-91-8,99108-56-2
morpholine

: 3762-25-2
diethyl 4-methylbenzylphosphonate

: 139546-54-6
4-(4-Methylselenobenzoyl)morpholine

Guidance literature:: With OC₄H₈N-(Se)n-NC₄H₈O (4, n=2,3,4); sodium hydride; Yield given. Multistep reaction; 1.) THF, 1 h, 2.) reflux, 7 h;
DOI:10.1246/cl.1992.131