C₃₅H₄₂O₆Si

Base Information

Chemical Name:C₃₅H₄₂O₆Si
CAS No.:1255639-83-8
Molecular Formula:C₃₅H₄₂O₆Si
Molecular Weight:586.8
Hs Code.:

C<sub>35</sub>H<sub>42</sub>O<sub>6</sub>Si

Synonyms:

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Chemical Property of C₃₅H₄₂O₆Si

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Technology Process of C₃₅H₄₂O₆Si

There total 11 articles about C₃₅H₄₂O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1255639-82-7
C₃₅H₄₂O₆Si

: 1255639-83-8
C₃₅H₄₂O₆Si

Guidance literature:: In chloroform-d1; for 96h; Inert atmosphere;
DOI:10.1021/ml1001807

Reference yield:

: 1255639-74-7
C₂₂H₂₈O₂Si

: 1255639-83-8
C₃₅H₄₂O₆Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: n-butyllithium / tetrahydrofuran / -78 - -10 °C / Inert atmosphere

1.2: -78 - 20 °C / Inert atmosphere

2.1: 1H-imidazole / N,N-dimethyl-formamide / 15 h / 20 °C / Inert atmosphere

3.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 5 h / 20 °C / Inert atmosphere

3.2: Inert atmosphere

3.3: 19 h / Inert atmosphere; Reflux

4.1: hydrogen / ethyl acetate / 0.83 h / 5625.56 Torr / Inert atmosphere

5.1: methanol; water; sodium hydroxide / 21 h / 87 °C / Inert atmosphere

6.1: triphenylphosphine; diethylazodicarboxylate / toluene / 0 - 20 °C / Inert atmosphere

7.1: Jones reagent; potassium fluoride / acetone / 2 h / -10 °C / Inert atmosphere

8.1: chloroform-d1 / 96 h / Inert atmosphere

With 1H-imidazole; methanol; potassium fluoride; Jones reagent; n-butyllithium; water; hydrogen; 9-bora-bicyclo[3.3.1]nonane; triphenylphosphine; sodium hydroxide; diethylazodicarboxylate; In tetrahydrofuran; chloroform-d1; ethyl acetate; N,N-dimethyl-formamide; acetone; toluene; 3.1: Suzuki Miyaura coupling / 3.2: Suzuki Miyaura coupling / 3.3: Suzuki Miyaura coupling / 6.1: Mitsunobu reaction;
DOI:10.1021/ml1001807

Reference yield:

: 1255639-73-6
(S)-3-(tert-butyldiphenylsiloxy)hex-5-en-1-ol

: 1255639-83-8
C₃₅H₄₂O₆Si

Guidance literature:: Multi-step reaction with 9 steps

1.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1 h / -78 °C / Inert atmosphere

1.2: -78 - 20 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran / -78 - -10 °C / Inert atmosphere

2.2: -78 - 20 °C / Inert atmosphere

3.1: 1H-imidazole / N,N-dimethyl-formamide / 15 h / 20 °C / Inert atmosphere

4.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 5 h / 20 °C / Inert atmosphere

4.2: Inert atmosphere

4.3: 19 h / Inert atmosphere; Reflux

5.1: hydrogen / ethyl acetate / 0.83 h / 5625.56 Torr / Inert atmosphere

6.1: methanol; water; sodium hydroxide / 21 h / 87 °C / Inert atmosphere

7.1: triphenylphosphine; diethylazodicarboxylate / toluene / 0 - 20 °C / Inert atmosphere

8.1: Jones reagent; potassium fluoride / acetone / 2 h / -10 °C / Inert atmosphere

9.1: chloroform-d1 / 96 h / Inert atmosphere

With 1H-imidazole; methanol; potassium fluoride; Jones reagent; n-butyllithium; oxalyl dichloride; water; hydrogen; dimethyl sulfoxide; 9-bora-bicyclo[3.3.1]nonane; triphenylphosphine; sodium hydroxide; diethylazodicarboxylate; In tetrahydrofuran; chloroform-d1; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; acetone; toluene; 1.1: Swern oxidation / 1.2: Swern oxidation / 4.1: Suzuki Miyaura coupling / 4.2: Suzuki Miyaura coupling / 4.3: Suzuki Miyaura coupling / 7.1: Mitsunobu reaction;
DOI:10.1021/ml1001807