Technology Process of 1-methyl-4-(4,4,5,5-tetramethyl-3-oxide-1-oxyl-4,5-dihydro-1H-imidazol-2-yl)-1H-pyrazolebis(4-imino-1,1,1,3,5,5,5-heptafluoropent-2-ene-2-aminato)copper(II) toluene monosolvate
There total 1 articles about 1-methyl-4-(4,4,5,5-tetramethyl-3-oxide-1-oxyl-4,5-dihydro-1H-imidazol-2-yl)-1H-pyrazolebis(4-imino-1,1,1,3,5,5,5-heptafluoropent-2-ene-2-aminato)copper(II) toluene monosolvate which
guide to synthetic route it.
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synthetic route:
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1346672-31-8
1-methyl-4-(4,4,5,5-tetramethyl-3-oxide-1-oxyl-4,5-dihydro-1H-imidazol-2-yl)-1H-pyrazolebis(4-imino-1,1,1,3,5,5,5-heptafluoropent-2-ene-2-aminato)copper(II) toluene monosolvate
- Guidance literature:
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In
diethyl ether; toluene;
soln. of nitroxide radical in toluene was added to soln. of Cu complex in ether; soln. vol. was decreased by passing a weak Ar flow above surface of mixt.; after 1 h crystals were obtained; filtered off; washed (cold toluene); dried (air); elem. anal.;
DOI:10.1007/s11172-011-0130-y