[PhP(CH₂SiMe₂NPh₂)]HoCl(THF)

Base Information

• Chemical Name: [PhP(CH₂SiMe₂NPh₂)]HoCl(THF)
• CAS No.: 375810-16-5
• Molecular Formula: C₂₈H₃₉ClHoN₂OPSi₂
• Molecular Weight: 707.159
• Mol file: 375810-16-5.mol

Synonyms:

Chemical Property of [PhP(CH₂SiMe₂NPh₂)]HoCl(THF)

Chemical Property:

Purity/Quality:

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Technology Process of [PhP(CH₂SiMe₂NPh₂)]HoCl(THF)

There total 1 articles about [PhP(CH₂SiMe₂NPh₂)]HoCl(THF) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

HoCl3(tetrahydrofuran)3 + (PhP(CH2SiMe2NPh)2)Li2*(THF)2 (215432-43-2) → [PhP(CH2SiMe2NPh2)]HoCl(THF) (375810-16-5)

Guidance literature:

In toluene; byproducts: LiCl; toluene added to equimolar mixt. of lithiated ligand precursor and lanthanide deriv. at room temp.; heated under reflux overnight; cooled to room temp., filtered through Celite; solvent evapd. to dryness; residue washed with hexane and dried under vac.; elem. anal.;

DOI:10.1139/v01-087

upstream raw materials:

(PhP(CH₂SiMe₂NPh)2)Li₂*(THF)2