C₂₉H₃₄N₄O₇

Base Information

Chemical Name:C₂₉H₃₄N₄O₇
CAS No.:1380315-91-2
Molecular Formula:C₂₉H₃₄N₄O₇
Molecular Weight:550.612
Hs Code.:

C<sub>29</sub>H<sub>34</sub>N<sub>4</sub>O<sub>7</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₉H₃₄N₄O₇

Chemical Property:

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Technology Process of C₂₉H₃₄N₄O₇

There total 7 articles about C₂₉H₃₄N₄O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 1380315-86-5
(3R,3'R)-di-tert-butyl,3'-bis(2-(methoxycarbonylamino)ethyl)-2,2'-dioxo-3,3'-biindoline-1,1'-dicarboxylate

: 1380315-91-2
C₂₉H₃₄N₄O₇

: 1380315-89-8
C₃₃H₄₂N₄O₆

: C₃₄H₄₄N₄O₁₀

Guidance literature:: (3R,3'R)-di-tert-butyl,3'-bis(2-(methoxycarbonylamino)ethyl)-2,2'-dioxo-3,3'-biindoline-1,1'-dicarboxylate; With lithium triethylborohydride; In tetrahydrofuran;

With hydrogenchloride; In tetrahydrofuran;
DOI:10.1002/anie.201201132

Reference yield:

: 1380315-88-7
di-tert-butyl 2,2′-dioxo-[3,3′-biindoline]-1,1′-dicarboxylate

: 1380315-91-2
C₂₉H₃₄N₄O₇

: 1380315-89-8
C₃₃H₄₂N₄O₆

: C₃₄H₄₄N₄O₁₀

Guidance literature:: Multi-step reaction with 3 steps

1.1: 2C₇H₄FO₂^(1-)*C₃₄H₂₀Mn₂N₂O₄⁽²⁺⁾ / toluene / 1.5 h / 50 °C / Molecular sieve; Inert atmosphere

1.2: 12 h / 50 °C / Molecular sieve; Inert atmosphere

2.1: sodium tetrahydroborate; nickel dichloride / methanol / 0 - 20 °C

3.1: lithium triethylborohydride / tetrahydrofuran

With sodium tetrahydroborate; 2C₇H₄FO₂^(1-)*C₃₄H₂₀Mn₂N₂O₄⁽²⁺⁾; lithium triethylborohydride; nickel dichloride; In tetrahydrofuran; methanol; toluene; 1.1: Michael reaction;
DOI:10.1002/anie.201201132

Reference yield:

: C₂₆H₂₆N₂O₆

: 1380315-91-2
C₂₉H₃₄N₄O₇

: 1380315-89-8
C₃₃H₄₂N₄O₆

: C₃₄H₄₄N₄O₁₀

Guidance literature:: Multi-step reaction with 4 steps

1.1: platinum(IV) oxide; hydrogen / dichloromethane; ethyl acetate / 12 h / 20 °C / 760.05 Torr / Inert atmosphere

2.1: 2C₇H₄FO₂^(1-)*C₃₄H₂₀Mn₂N₂O₄⁽²⁺⁾ / toluene / 1.5 h / 50 °C / Molecular sieve; Inert atmosphere

2.2: 12 h / 50 °C / Molecular sieve; Inert atmosphere

3.1: sodium tetrahydroborate; nickel dichloride / methanol / 0 - 20 °C

4.1: lithium triethylborohydride / tetrahydrofuran

With platinum(IV) oxide; sodium tetrahydroborate; 2C₇H₄FO₂^(1-)*C₃₄H₂₀Mn₂N₂O₄⁽²⁺⁾; hydrogen; lithium triethylborohydride; nickel dichloride; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate; toluene; 2.1: Michael reaction;
DOI:10.1002/anie.201201132