N'-benzylbenzohydrazonamide

Base Information

• Chemical Name: N'-benzylbenzohydrazonamide
• CAS No.: 1357310-09-8
• Molecular Formula: C₁₄H₁₅N₃
• Molecular Weight: 225.293
• Mol file: 1357310-09-8.mol

Synonyms:

Chemical Property of N'-benzylbenzohydrazonamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N'-benzylbenzohydrazonamide

There total 1 articles about N'-benzylbenzohydrazonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

benzimidic acid ethyl ester (825-60-5) + Benzylhydrazine (555-96-4) → N'-benzylbenzohydrazonamide (1357310-09-8)

Guidance literature:

In ethanol; at 30 - 40 ℃; for 4h;

DOI:10.1016/j.tetlet.2011.09.049

Reference yield:

N'-benzylbenzohydrazonamide (1357310-09-8) → C20H16N4 (1346229-79-5)

Guidance literature:

Multi-step reaction with 2 steps

1: toluene / 10 h / 110 - 120 °C

2: palladium on activated charcoal; hydrazine hydrochloride; sodium hydroxide / toluene / 24 h / 25 °C

With hydrazine hydrochloride; palladium on activated charcoal; sodium hydroxide; In toluene;

DOI:10.1016/j.tetlet.2011.09.049

Reference yield:

N'-benzylbenzohydrazonamide (1357310-09-8) → C27H22N4O (1346229-80-8)

Guidance literature:

Multi-step reaction with 2 steps

1: toluene / 10 h / 110 - 120 °C

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydrogencarbonate / N,N-dimethyl-formamide / 0.25 h / Microwave irradiation

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydrogencarbonate; In N,N-dimethyl-formamide; toluene; 2: Suzuki coupling;

DOI:10.1016/j.tetlet.2011.09.049

upstream raw materials:

benzimidic acid ethyl ester

Benzylhydrazine

Downstream raw materials:

C₂₀H₁₆N₄

C₁₉H₁₅N₅

C₂₀H₁₅BrN₄

C₂₀H₁₆N₄