C₁₇H₂₂O₅S

Base Information

• Chemical Name: C₁₇H₂₂O₅S
• CAS No.: 1356956-17-6
• Molecular Formula: C₁₇H₂₂O₅S
• Molecular Weight: 338.425
• Mol file: 1356956-17-6.mol

Synonyms:

Chemical Property of C₁₇H₂₂O₅S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₇H₂₂O₅S

There total 4 articles about C₁₇H₂₂O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

acetic acid (1S,6R)-6-hydroxymethyl-cyclohex-3-enylmethyl ester (98516-11-1,118014-45-2,98516-10-0) + p-toluenesulfonyl chloride (98-59-9) → C17H22O5S (1356956-17-6)

Guidance literature:

acetic acid (1S,6R)-6-hydroxymethyl-cyclohex-3-enylmethyl ester; p-toluenesulfonyl chloride; With pyridine; In dichloromethane; at 0 ℃; for 1h; Inert atmosphere;

With 1-methyl-piperazine; In dichloromethane; at 20 ℃; for 0.333333h; Inert atmosphere;

DOI:10.1021/ja3111626

Reference yield:

cis-1,2,3,6-tetrahydrophthalic anhydride (935-79-5) → C17H22O5S (1356956-17-6)

Guidance literature:

Multi-step reaction with 3 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 4.17 h / 0 °C / Inert atmosphere

2.1: porcine pancreatic lipase / 120 h / 20 °C / Inert atmosphere; Molecular sieve; Enzymatic reaction

3.1: pyridine / dichloromethane / 1 h / 0 °C / Inert atmosphere

3.2: 0.33 h / 20 °C / Inert atmosphere

With pyridine; lithium aluminium tetrahydride; In tetrahydrofuran; dichloromethane;

DOI:10.1021/ja3111626

Reference yield:

cis-1,6-dihydroxymethyl-3-cyclohexene (439919-46-7) → C17H22O5S (1356956-17-6)

Guidance literature:

Multi-step reaction with 2 steps

1.1: porcine pancreatic lipase / 120 h / 20 °C / Inert atmosphere; Molecular sieve; Enzymatic reaction

2.1: pyridine / dichloromethane / 1 h / 0 °C / Inert atmosphere

2.2: 0.33 h / 20 °C / Inert atmosphere

With pyridine; In dichloromethane;

DOI:10.1021/ja3111626

upstream raw materials:

acetic acid methyl ester

cis-1,6-dihydroxymethyl-3-cyclohexene

p-toluenesulfonyl chloride

cis-1,2,3,6-tetrahydrophthalic anhydride

Downstream raw materials:

C₁₁H₁₅NO₂