propanoyltriphenylgermane

Base Information

• Chemical Name: propanoyltriphenylgermane
• CAS No.: 105028-39-5
• Molecular Formula: C₂₁H₂₀GeO
• Molecular Weight: 360.979
• Mol file: 105028-39-5.mol

Synonyms:

Chemical Property of propanoyltriphenylgermane

Chemical Property:

Purity/Quality:

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Useful:

Technology Process of propanoyltriphenylgermane

There total 1 articles about propanoyltriphenylgermane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

triphenylgermyl lithium (3839-32-5) + Ethyl propionate (105-37-3,20741-13-3) → propanoyltriphenylgermane (105028-39-5)

Guidance literature:

In tetrahydrofuran; byproducts: LiOC2H5, Ge(C6H5)3H; dropwise addn. of organic compd. (via syringe) to a soln. of Li-compd. (prepd. from GePh3 and BuLi in hexane) at room temp. under Ar, stirred for 10 min; quenched with aq. NH4Cl, organic layer extd. (ether), dried over MgSO4, evapd., flash chromy.;

DOI:10.1246/cl.1985.1829

upstream raw materials:

triphenylgermyl lithium

Ethyl propionate

Refernces