C₄₃H₅₇N₅O₁₁

Base Information

Chemical Name:C₄₃H₅₇N₅O₁₁
CAS No.:1393358-79-6
Molecular Formula:C₄₃H₅₇N₅O₁₁
Molecular Weight:819.952
Hs Code.:

C<sub>43</sub>H<sub>57</sub>N<sub>5</sub>O<sub>11</sub>

Synonyms:

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Chemical Property of C₄₃H₅₇N₅O₁₁

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Technology Process of C₄₃H₅₇N₅O₁₁

There total 6 articles about C₄₃H₅₇N₅O₁₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 1393358-78-5
C₁₇H₂₁NO₆

: 1393358-75-2
C₂₆H₃₈N₄O₆

: 1393358-79-6
C₄₃H₅₇N₅O₁₁

Guidance literature:: C₁₇H₂₁NO₆; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; at 0 ℃; for 0.0833333h;

C₂₆H₃₈N₄O₆; With dmap; triethylamine; In tetrahydrofuran; at 20 ℃; for 6h;
DOI:10.1002/jps.23109

Reference yield:

: 1393358-71-8
C₁₃H₂₂N₂O₅

: 1393358-79-6
C₄₃H₅₇N₅O₁₁

Guidance literature:: Multi-step reaction with 6 steps

1.1: hydrogenchloride / ethyl acetate / 0.5 h / 0 °C

2.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / tetrahydrofuran / 0.08 h / Cooling with ice

2.2: 5 h / 20 °C

3.1: morpholine; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran / 1.5 h / 20 °C

4.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / tetrahydrofuran / 0.08 h / Cooling with ice

4.2: 5 h / 20 °C

5.1: hydrogenchloride / ethyl acetate / 0.5 h / 0 °C

6.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / tetrahydrofuran / 0.08 h / 0 °C

6.2: 6 h / 20 °C

With morpholine; hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; ethyl acetate;
DOI:10.1002/jps.23109

Reference yield:

: 3744-87-4,7764-95-6,15761-38-3
Boc-(R)-Ala

: 1393358-79-6
C₄₃H₅₇N₅O₁₁

Guidance literature:: Multi-step reaction with 4 steps

1.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.08 h / 0 °C

1.2: 5 h / 0 °C

2.1: quinoline; Pb-poisoned 5% Pd-CaCO3; hydrogen / 0.5 h / 0 °C

3.1: acetic acid; zinc / 0.5 h / 10 °C

4.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / tetrahydrofuran / 0.08 h / 0 °C

4.2: 6 h / 20 °C

With quinoline; dmap; Pb-poisoned 5% Pd-CaCO3; hydrogen; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; zinc; In tetrahydrofuran; dichloromethane;
DOI:10.1002/jps.23109