N-acetyl (2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-(1->3)-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-acetyl-β-D-glucopyranoside

Base Information

Chemical Name:N-acetyl (2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-(1->3)-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-acetyl-β-D-glucopyranoside
CAS No.:252845-51-5
Molecular Formula:C₆₀H₇₁NO₂₂
Molecular Weight:1158.22
Hs Code.:

N-acetyl (2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-(1->3)-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-acetyl-β-D-glucopyranoside

Synonyms:

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Chemical Property of N-acetyl (2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-(1->3)-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-acetyl-β-D-glucopyranoside

Chemical Property:

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Safty Information:

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Technology Process of N-acetyl (2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-(1->3)-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-acetyl-β-D-glucopyranoside

There total 7 articles about N-acetyl (2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-(1->3)-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-acetyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 226707-92-2
O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-acetyl-1-β-D-glucopyranosyl azide

: 252845-51-5
N-acetyl (2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-(1->3)-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-acetyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

2: hydrogen / PtO₂ / ethanol / 1 h / 2068.59 Torr

3: 86 mg / triethylamine / CH₂Cl₂ / 0 - 20 °C

With hydrogen; triethylamine; platinum(IV) oxide; In ethanol; dichloromethane; 1: glycosylation / 2: Hydrogenolysis / 3: Acetylation;
DOI:10.1080/07328309908544050

Reference yield:

: 252845-50-4
[3-O-(4-methoxybenzyl) 2,4,6-tri-O-acetyl-β-D-galactopyranosyl]-(1->4)-2,3,6-tri-O-acetyl-β-D-glucopyranosyl azide

: 252845-51-5
N-acetyl (2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-(1->3)-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-acetyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / cerium(IV) ammonium nitrate / acetonitrile; H₂O / 0 - 10 °C

3: hydrogen / PtO₂ / ethanol / 1 h / 2068.59 Torr

4: 86 mg / triethylamine / CH₂Cl₂ / 0 - 20 °C

With ammonium cerium(IV) nitrate; hydrogen; triethylamine; platinum(IV) oxide; In ethanol; dichloromethane; water; acetonitrile; 1: Oxidation / 2: glycosylation / 3: Hydrogenolysis / 4: Acetylation;
DOI:10.1080/07328309908544050

Reference yield:

: 97205-08-8,162061-34-9
methyl 2,3,4,6-tetra-O-benzyl-1-thio-β-D-galactopyranoside

: 252845-51-5
N-acetyl (2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-(1->3)-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-acetyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

2: hydrogen / PtO₂ / ethanol / 1 h / 2068.59 Torr

3: 86 mg / triethylamine / CH₂Cl₂ / 0 - 20 °C

With hydrogen; triethylamine; platinum(IV) oxide; In ethanol; dichloromethane; 1: glycosylation / 2: Hydrogenolysis / 3: Acetylation;
DOI:10.1080/07328309908544050