Technology Process of C36H39Cl3N4O4S
There total 3 articles about C36H39Cl3N4O4S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
bis{rhodium[3,3'-(1,3-phenylene)bis(2,2-dimethylpropanoic acid)]}; bis(tertbutylcarbonyloxy)iodobenzene;
In
benzene;
at 23 ℃;
for 0.5h;
Overall yield = 21 %;
Inert atmosphere;
DOI:10.1038/nchem.1653
- Guidance literature:
-
Multi-step reaction with 2 steps
1: isocyanate de chlorosulfonyle; formic acid / acetonitrile; N,N-dimethyl acetamide / 0 - 23 °C
2: bis(tertbutylcarbonyloxy)iodobenzene; bis{rhodium[3,3'-(1,3-phenylene)bis(2,2-dimethylpropanoic acid)]} / benzene / 0.5 h / 23 °C / Inert atmosphere
With
formic acid; isocyanate de chlorosulfonyle; bis{rhodium[3,3'-(1,3-phenylene)bis(2,2-dimethylpropanoic acid)]}; bis(tertbutylcarbonyloxy)iodobenzene;
In
N,N-dimethyl acetamide; acetonitrile; benzene;
DOI:10.1038/nchem.1653
- Guidance literature:
-
Multi-step reaction with 3 steps
1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 23 °C
2: isocyanate de chlorosulfonyle; formic acid / acetonitrile; N,N-dimethyl acetamide / 0 - 23 °C
3: bis(tertbutylcarbonyloxy)iodobenzene; bis{rhodium[3,3'-(1,3-phenylene)bis(2,2-dimethylpropanoic acid)]} / benzene / 0.5 h / 23 °C / Inert atmosphere
With
formic acid; isocyanate de chlorosulfonyle; bis{rhodium[3,3'-(1,3-phenylene)bis(2,2-dimethylpropanoic acid)]}; bis(tertbutylcarbonyloxy)iodobenzene; N-ethyl-N,N-diisopropylamine;
In
dichloromethane; N,N-dimethyl acetamide; acetonitrile; benzene;
DOI:10.1038/nchem.1653
