((CH₃)3SiO)2C₆H₃NCW(CO)5

Base Information

Chemical Name:((CH₃)3SiO)2C₆H₃NCW(CO)5
CAS No.:666748-12-5
Molecular Formula:C₁₈H₂₁NO₇Si₂W
Molecular Weight:603.388
Hs Code.:

((CH<sub>3</sub>)3SiO)2C<sub>6</sub>H<sub>3</sub>NCW(CO)5

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ((CH₃)3SiO)2C₆H₃NCW(CO)5

Chemical Property:

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Technology Process of ((CH₃)3SiO)2C₆H₃NCW(CO)5

There total 2 articles about ((CH₃)3SiO)2C₆H₃NCW(CO)5 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 14040-11-0
tungsten hexacarbonyl

: 666748-12-5
((CH₃)3SiO)2C₆H₃NCW(CO)5

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran

2: tetrahydrofuran

In tetrahydrofuran;
DOI:10.1002/zaac.200300078

Reference yield:

: 36477-75-5
tungsten pentacarbonyl tetrahydrofuran

: 166329-37-9
2,6-bis(trimethylsiloxy)phenyl isocyanide

: 666748-12-5
((CH₃)3SiO)2C₆H₃NCW(CO)5

Guidance literature:: In tetrahydrofuran; all manipulations under Ar; org. compd. added dropwise to soln. of W compd., stirred overnight; solvent removed, crude product isolated;
DOI:10.1002/zaac.200300078

Reference yield:

: 666748-12-5
((CH₃)3SiO)2C₆H₃NCW(CO)5

: 666748-20-5
2,6-dihydroxyphenyl-isocyanidepentacarbonyl tungsten

: (4-hydroxybenzoxazol-2-ylidene)pentacarbonyl tungsten

Guidance literature:: With KF; In methanol; all manipulations under Ar; crude compd. dissolved in MeOH, KF added, stirred at room temp. for 3 d, equil. reaction; evapd. to dryness, chromy. (Al2O3, 3% H2O, MeOH/Et2O 1/1, v/v), only 3:1mixt. of products isolated;
DOI:10.1002/zaac.200300078