C₄₄H₅₇ClO₉

Base Information

Chemical Name:C₄₄H₅₇ClO₉
CAS No.:616200-85-2
Molecular Formula:C₄₄H₅₇ClO₉
Molecular Weight:765.384
Hs Code.:

C<sub>44</sub>H<sub>57</sub>ClO<sub>9</sub>

Synonyms:

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Chemical Property of C₄₄H₅₇ClO₉

Chemical Property:

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Technology Process of C₄₄H₅₇ClO₉

There total 7 articles about C₄₄H₅₇ClO₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 971-93-7
tri-p-tolylmethylchloride

: 616200-85-2
C₄₄H₅₇ClO₉

Guidance literature:: Multi-step reaction with 7 steps

1: 10.2 g / 18 h / 100 °C

2: 2,6-dimethylpyridine; DMAP / CH₂Cl₂ / 1.5 h / -30 - 20 °C

3: 14.2 g / Et₃N; 1,3-bis(diphenylphosphino)propane / Pd(OAc)2 / dimethylformamide; methanol / 7 h / 70 °C

4: NBS; AIBN / CCl₄ / 6 h / Heating

5: 15-crown-5; NaI; NaH / tetrahydrofuran / 20 h / Heating

6: 2.05 g / LiAlH₄ / tetrahydrofuran / 24 h / 20 °C

7: 99 percent / SOCl₂ / CH₂Cl₂ / 2 h / 20 °C

With 2,6-dimethylpyridine; dmap; N-Bromosuccinimide; lithium aluminium tetrahydride; thionyl chloride; 15-crown-5; 2,2'-azobis(isobutyronitrile); 1,3-bis-(diphenylphosphino)propane; sodium hydride; triethylamine; sodium iodide; palladium diacetate; In tetrahydrofuran; methanol; tetrachloromethane; dichloromethane; N,N-dimethyl-formamide; 1: Friedel-Crafts reaction;
DOI:10.1135/cccc20031488

Reference yield:

: 3247-00-5
tris(4-methylphenyl)methanol

: 616200-85-2
C₄₄H₅₇ClO₉

Guidance literature:: Multi-step reaction with 8 steps

1: AcCl / 24 h / Heating

2: 10.2 g / 18 h / 100 °C

3: 2,6-dimethylpyridine; DMAP / CH₂Cl₂ / 1.5 h / -30 - 20 °C

4: 14.2 g / Et₃N; 1,3-bis(diphenylphosphino)propane / Pd(OAc)2 / dimethylformamide; methanol / 7 h / 70 °C

5: NBS; AIBN / CCl₄ / 6 h / Heating

6: 15-crown-5; NaI; NaH / tetrahydrofuran / 20 h / Heating

7: 2.05 g / LiAlH₄ / tetrahydrofuran / 24 h / 20 °C

8: 99 percent / SOCl₂ / CH₂Cl₂ / 2 h / 20 °C

With 2,6-dimethylpyridine; dmap; N-Bromosuccinimide; lithium aluminium tetrahydride; thionyl chloride; 15-crown-5; 2,2'-azobis(isobutyronitrile); 1,3-bis-(diphenylphosphino)propane; sodium hydride; triethylamine; acetyl chloride; sodium iodide; palladium diacetate; In tetrahydrofuran; methanol; tetrachloromethane; dichloromethane; N,N-dimethyl-formamide; 2: Friedel-Crafts reaction;
DOI:10.1135/cccc20031488

Reference yield:

: trifluoro-methanesulfonic acid 4-tri-p-tolylmethyl-phenyl ester

: 616200-85-2
C₄₄H₅₇ClO₉

Guidance literature:: Multi-step reaction with 5 steps

1: 14.2 g / Et₃N; 1,3-bis(diphenylphosphino)propane / Pd(OAc)2 / dimethylformamide; methanol / 7 h / 70 °C

2: NBS; AIBN / CCl₄ / 6 h / Heating

3: 15-crown-5; NaI; NaH / tetrahydrofuran / 20 h / Heating

4: 2.05 g / LiAlH₄ / tetrahydrofuran / 24 h / 20 °C

5: 99 percent / SOCl₂ / CH₂Cl₂ / 2 h / 20 °C

With N-Bromosuccinimide; lithium aluminium tetrahydride; thionyl chloride; 15-crown-5; 2,2'-azobis(isobutyronitrile); 1,3-bis-(diphenylphosphino)propane; sodium hydride; triethylamine; sodium iodide; palladium diacetate; In tetrahydrofuran; methanol; tetrachloromethane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1135/cccc20031488