C₂₂H₁₈⁽²⁾H₃NO₃

Base Information

• Chemical Name: C₂₂H₁₈⁽²⁾H₃NO₃
• CAS No.: 1607800-92-9
• Molecular Formula: C₂₂H₂₁NO₃
• Molecular Weight: 350.39
• Mol file: 1607800-92-9.mol

Synonyms:

Chemical Property of C₂₂H₁₈⁽²⁾H₃NO₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of C₂₂H₁₈⁽²⁾H₃NO₃

There total 1 articles about C₂₂H₁₈⁽²⁾H₃NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-tert-butyloxycarbonyl-pyrrole (5176-27-2) + N-boc-pyrrole (1607800-91-8) + (4-aminophenyl)(phenyl)methanone (1137-41-3,444317-48-0) → N-tert-butoxycarbonyl-2-(4-benzoylphenyl)-1H-pyrrole (1607800-83-8) + C22H18(2)H3NO3 (1607800-92-9)

Guidance literature:

(4-aminophenyl)(phenyl)methanone; With tert.-butylnitrite; methanesulfonic acid; In water; at 25 ℃; for 0.5h;

N-tert-butyloxycarbonyl-pyrrole; N-boc-pyrrole; With copper(II) acetate monohydrate; calcium carbonate; In water; acetone; at 25 ℃; for 3h; Overall yield = 73 %; regioselective reaction;

DOI:10.1039/c3cc45240a

upstream raw materials:

N-tert-butyloxycarbonyl-pyrrole

N-boc-pyrrole

(4-aminophenyl)(phenyl)methanone