C₃₉H₅₃F₂N₇O₅Si

Base Information

Chemical Name:C₃₉H₅₃F₂N₇O₅Si
CAS No.:1659311-08-6
Molecular Formula:C₃₉H₅₃F₂N₇O₅Si
Molecular Weight:765.976
Hs Code.:

C<sub>39</sub>H<sub>53</sub>F<sub>2</sub>N<sub>7</sub>O<sub>5</sub>Si

Synonyms:

Suppliers and Price of C₃₉H₅₃F₂N₇O₅Si

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₃₉H₅₃F₂N₇O₅Si

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₃₉H₅₃F₂N₇O₅Si

There total 14 articles about C₃₉H₅₃F₂N₇O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1210418-60-2
tert-butyl (4R)-4-((1R,2S)-1-{[tert-butyl(dimethyl)silyl]oxy}-3-hydroxy-2-methylpropyl)-2,2-dimethyl-1,3-oxazolidine-3-carboxylate

: 1659311-08-6
C₃₉H₅₃F₂N₇O₅Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: di-isopropyl azodicarboxylate; triphenylphosphine; diphenyl phosphoryl azide / tetrahydrofuran / 20 °C

2.1: pyridinium p-toluenesulfonate / ethanol / 48 h / Reflux

2.2: 3 h / 20 °C

3.1: pyridine; dmap / 1 h / 0 °C

4.1: palladium 10% on activated carbon; hydrogen; N-ethyl-N,N-diisopropylamine / methanol / 2 h

5.1: N-ethyl-N,N-diisopropylamine / isopropyl alcohol / 2 h / 60 °C

6.1: palladium 10% on activated carbon; hydrogen / methanol / 3 h

7.1: tetrahydrofuran / 2 h / 60 °C

8.1: trimethylphosphane / tetrahydrofuran / 0.25 h / 20 °C

8.2: 0.25 h / 20 °C

With pyridine; dmap; di-isopropyl azodicarboxylate; diphenyl phosphoryl azide; palladium 10% on activated carbon; hydrogen; pyridinium p-toluenesulfonate; N-ethyl-N,N-diisopropylamine; triphenylphosphine; trimethylphosphane; In tetrahydrofuran; methanol; ethanol; isopropyl alcohol;

Reference yield:

: 1210418-61-3
tert-butyl (4R)-4-((1R,2S)-3-azido-1-{[tert-butyl(dimethyl)silyl]oxy}-2-methylpropyl)-2,2-dimethyl-1,3-oxazolidine-3-carboxylate

: 1659311-08-6
C₃₉H₅₃F₂N₇O₅Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: pyridinium p-toluenesulfonate / ethanol / 48 h / Reflux

1.2: 3 h / 20 °C

2.1: pyridine; dmap / 1 h / 0 °C

3.1: palladium 10% on activated carbon; hydrogen; N-ethyl-N,N-diisopropylamine / methanol / 2 h

4.1: N-ethyl-N,N-diisopropylamine / isopropyl alcohol / 2 h / 60 °C

5.1: palladium 10% on activated carbon; hydrogen / methanol / 3 h

6.1: tetrahydrofuran / 2 h / 60 °C

7.1: trimethylphosphane / tetrahydrofuran / 0.25 h / 20 °C

7.2: 0.25 h / 20 °C

With pyridine; dmap; palladium 10% on activated carbon; hydrogen; pyridinium p-toluenesulfonate; N-ethyl-N,N-diisopropylamine; trimethylphosphane; In tetrahydrofuran; methanol; ethanol; isopropyl alcohol;

Reference yield:

: 1210418-63-5
(R)-tert-butyl 4-((1R,2S)-3-azido-1-(tert-butyldimethylsilyloxy)-2-methylpropyl)-2,2-dimethyloxazolidine-3-carboxylate

: 1659311-08-6
C₃₉H₅₃F₂N₇O₅Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: pyridine; dmap / 1 h / 0 °C

2.1: palladium 10% on activated carbon; hydrogen; N-ethyl-N,N-diisopropylamine / methanol / 2 h

3.1: N-ethyl-N,N-diisopropylamine / isopropyl alcohol / 2 h / 60 °C

4.1: palladium 10% on activated carbon; hydrogen / methanol / 3 h

5.1: tetrahydrofuran / 2 h / 60 °C

6.1: trimethylphosphane / tetrahydrofuran / 0.25 h / 20 °C

6.2: 0.25 h / 20 °C

With pyridine; dmap; palladium 10% on activated carbon; hydrogen; N-ethyl-N,N-diisopropylamine; trimethylphosphane; In tetrahydrofuran; methanol; isopropyl alcohol;