Technology Process of C35H54O21S
There total 7 articles about C35H54O21S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
silver nitrate;
In
methanol;
at 20 ℃;
for 24h;
stereoselective reaction;
Inert atmosphere;
Darkness;
DOI:10.1021/jo102411j
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 12 h / 20 °C
2.1: dichloromethane / 0.5 h / 20 °C / Molecular sieve
2.2: 12 h / 20 °C / Molecular sieve
3.1: acetic acid / water
4.1: methanol; sodium / Inert atmosphere
5.1: methanol / 20 °C / Inert atmosphere
6.1: silver nitrate / methanol / 24 h / 20 °C / Inert atmosphere; Darkness
With
methanol; sodium; silver nitrate; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene;
In
methanol; dichloromethane; water;
DOI:10.1021/jo102411j
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: hydrazinium monoacetate / N,N-dimethyl-formamide / 20 °C
2.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 12 h / 20 °C
3.1: dichloromethane / 0.5 h / 20 °C / Molecular sieve
3.2: 12 h / 20 °C / Molecular sieve
4.1: acetic acid / water
5.1: methanol; sodium / Inert atmosphere
6.1: methanol / 20 °C / Inert atmosphere
7.1: silver nitrate / methanol / 24 h / 20 °C / Inert atmosphere; Darkness
With
methanol; sodium; hydrazinium monoacetate; silver nitrate; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene;
In
methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/jo102411j
