C₂₃H₃₆F₄N₂O₅S

Base Information

Chemical Name:C₂₃H₃₆F₄N₂O₅S
CAS No.:1455445-95-0
Molecular Formula:C₂₃H₃₆F₄N₂O₅S
Molecular Weight:528.609
Hs Code.:

C<sub>23</sub>H<sub>36</sub>F<sub>4</sub>N<sub>2</sub>O<sub>5</sub>S

Synonyms:

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Chemical Property of C₂₃H₃₆F₄N₂O₅S

Chemical Property:

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Technology Process of C₂₃H₃₆F₄N₂O₅S

There total 8 articles about C₂₃H₃₆F₄N₂O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₃H₃₄F₄N₂O₇S

: 1455445-95-0
C₂₃H₃₆F₄N₂O₅S

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; at 45 ℃;
DOI:10.1016/j.bmcl.2013.07.071

Reference yield:

: 1204344-04-6
C₂₁H₂₈F₄N₂O₇S

: 1455445-95-0
C₂₃H₃₆F₄N₂O₅S

Guidance literature:: Multi-step reaction with 5 steps

1: dihydrogen peroxide / tetrahydrofuran; acetic acid / 6 h / 25 °C

2: trifluoroacetic acid / dichloromethane / 1 h / 25 °C

3: sodium acetate / dichloromethane; methanol / 2 h / 25 °C

4: sodium cyanoborohydride / methanol / 1 h / 25 °C

5: hydrogen; palladium 10% on activated carbon / methanol / 45 °C

With palladium 10% on activated carbon; hydrogen; dihydrogen peroxide; sodium acetate; sodium cyanoborohydride; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; acetic acid;
DOI:10.1016/j.bmcl.2013.07.071

Reference yield:

: 1123172-99-5
((3R,4S,5S)-5-(3,5-difluoro-4-nitrobenzyl)-4-hydroxy-1,1-dioxidotetrahydro-2H-thiopyran-3-yl)carbamate

: 1455445-95-0
C₂₃H₃₆F₄N₂O₅S

Guidance literature:: Multi-step reaction with 6 steps

1: potassium hydroxide / tetrahydrofuran / 24 h / 40 °C

2: dihydrogen peroxide / tetrahydrofuran; acetic acid / 6 h / 25 °C

3: trifluoroacetic acid / dichloromethane / 1 h / 25 °C

4: sodium acetate / dichloromethane; methanol / 2 h / 25 °C

5: sodium cyanoborohydride / methanol / 1 h / 25 °C

6: hydrogen; palladium 10% on activated carbon / methanol / 45 °C

With palladium 10% on activated carbon; hydrogen; dihydrogen peroxide; sodium acetate; sodium cyanoborohydride; trifluoroacetic acid; potassium hydroxide; In tetrahydrofuran; methanol; dichloromethane; acetic acid;
DOI:10.1016/j.bmcl.2013.07.071