(R)-2-[(S)-2-Amino-3-(4-hydroxy-phenyl)-propionylamino]-pentanedioic acid 1-({[(S)-2-(N'-acetyl-hydrazino)-1-benzyl-2-oxo-ethylcarbamoyl]-methyl}-amide) 5-amide

Base Information

Chemical Name:(R)-2-[(S)-2-Amino-3-(4-hydroxy-phenyl)-propionylamino]-pentanedioic acid 1-({[(S)-2-(N'-acetyl-hydrazino)-1-benzyl-2-oxo-ethylcarbamoyl]-methyl}-amide) 5-amide
CAS No.:74086-26-3
Molecular Formula:C₂₇H₃₅N₇O₇
Molecular Weight:569.618
Hs Code.:

(R)-2-[(S)-2-Amino-3-(4-hydroxy-phenyl)-propionylamino]-pentanedioic acid 1-({[(S)-2-(N'-acetyl-hydrazino)-1-benzyl-2-oxo-ethylcarbamoyl]-methyl}-amide) 5-amide

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Chemical Property of (R)-2-[(S)-2-Amino-3-(4-hydroxy-phenyl)-propionylamino]-pentanedioic acid 1-({[(S)-2-(N'-acetyl-hydrazino)-1-benzyl-2-oxo-ethylcarbamoyl]-methyl}-amide) 5-amide

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Technology Process of (R)-2-[(S)-2-Amino-3-(4-hydroxy-phenyl)-propionylamino]-pentanedioic acid 1-({[(S)-2-(N'-acetyl-hydrazino)-1-benzyl-2-oxo-ethylcarbamoyl]-methyl}-amide) 5-amide

There total 7 articles about (R)-2-[(S)-2-Amino-3-(4-hydroxy-phenyl)-propionylamino]-pentanedioic acid 1-({[(S)-2-(N'-acetyl-hydrazino)-1-benzyl-2-oxo-ethylcarbamoyl]-methyl}-amide) 5-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 74086-25-2
[(S)-1-[(R)-1-({[(S)-2-(N'-Acetyl-hydrazino)-1-benzyl-2-oxo-ethylcarbamoyl]-methyl}-carbamoyl)-3-carbamoyl-propylcarbamoyl]-2-(4-hydroxy-phenyl)-ethyl]-carbamic acid benzyl ester

: 74086-26-3
(R)-2-[(S)-2-Amino-3-(4-hydroxy-phenyl)-propionylamino]-pentanedioic acid 1-({[(S)-2-(N'-acetyl-hydrazino)-1-benzyl-2-oxo-ethylcarbamoyl]-methyl}-amide) 5-amide

Guidance literature:: With hydrogen; palladium; In methanol;
DOI:10.1248/cpb.29.3646

Reference yield:

: 74086-19-4
N-[(S)-2-(N'-Acetyl-hydrazino)-1-benzyl-2-oxo-ethyl]-2-amino-acetamide

: 74086-26-3
(R)-2-[(S)-2-Amino-3-(4-hydroxy-phenyl)-propionylamino]-pentanedioic acid 1-({[(S)-2-(N'-acetyl-hydrazino)-1-benzyl-2-oxo-ethylcarbamoyl]-methyl}-amide) 5-amide

Guidance literature:: Multi-step reaction with 4 steps

1: dimethylformamide / Ambient temperature

2: TFA / 0.33 h / Ambient temperature

3: dimethylformamide / Ambient temperature

4: hydrogen / Pd-black / methanol

With hydrogen; trifluoroacetic acid; palladium; In methanol; N,N-dimethyl-formamide;
DOI:10.1248/cpb.29.3646

Reference yield:

: 74086-18-3
{[(S)-2-(N'-Acetyl-hydrazino)-1-benzyl-2-oxo-ethylcarbamoyl]-methyl}-carbamic acid benzyl ester

: 74086-26-3
(R)-2-[(S)-2-Amino-3-(4-hydroxy-phenyl)-propionylamino]-pentanedioic acid 1-({[(S)-2-(N'-acetyl-hydrazino)-1-benzyl-2-oxo-ethylcarbamoyl]-methyl}-amide) 5-amide

Guidance literature:: Multi-step reaction with 5 steps

1: 3.5 mg / hydrogen / Pd-black / methanol

2: dimethylformamide / Ambient temperature

3: TFA / 0.33 h / Ambient temperature

4: dimethylformamide / Ambient temperature

5: hydrogen / Pd-black / methanol

With hydrogen; trifluoroacetic acid; palladium; In methanol; N,N-dimethyl-formamide;
DOI:10.1248/cpb.29.3646