6-(p-nitrophenyl)dibenz-1,3-oxazepine

Base Information

• Chemical Name: 6-(p-nitrophenyl)dibenz-1,3-oxazepine
• CAS No.: 116449-39-9
• Molecular Formula: C₁₉H₁₂N₂O₃
• Molecular Weight: 316.316
• Mol file: 116449-39-9.mol

Synonyms:

Chemical Property of 6-(p-nitrophenyl)dibenz-1,3-oxazepine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 6-(p-nitrophenyl)dibenz-1,3-oxazepine

There total 2 articles about 6-(p-nitrophenyl)dibenz-1,3-oxazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

6-(p-nitrophenyl)phenanthridine N-oxide (116449-36-6) → 6-(4-nitrophenyl)phenanthridine (98351-83-8) + 6-(p-nitrophenyl)dibenz-1,3-oxazepine (116449-39-9) + 2-(2-hydroxyphenyl)-N-(p-nitrobenzoyl)aniline (116449-43-5)

Guidance literature:

In benzene; at 17 ℃; Irradiation; with Helios quartz light;

DOI:10.1039/P29880000235

Reference yield:

6-(4-nitrophenyl)phenanthridine (98351-83-8) → 6-(p-nitrophenyl)dibenz-1,3-oxazepine (116449-39-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 89 percent / 40percent H₂O₂ / acetic acid / 4 h / 50 °C

2: 30 percent / benzene / 17 °C / Irradiation; with Helios quartz light

With dihydrogen peroxide; In acetic acid; benzene;

DOI:10.1039/P29880000235

upstream raw materials:

6-(p-nitrophenyl)phenanthridine N-oxide

6-(4-nitrophenyl)phenanthridine