14-Benzyloxycarbonyl-4-[5-benzyloxycarbonyl-4-(2-methoxycarbonylethyl)-3-(methoxycarbonylmethyl)pyrrol-2-ylmethyl]-2,8,13-tris(2-methoxycarbonylethyl)-3,7,12-tris(methoxycarbonylmethyl)-4,5-dihydrotripyrrin-1,10(15H,17H)-dithione

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Chemical Name:14-Benzyloxycarbonyl-4-[5-benzyloxycarbonyl-4-(2-methoxycarbonylethyl)-3-(methoxycarbonylmethyl)pyrrol-2-ylmethyl]-2,8,13-tris(2-methoxycarbonylethyl)-3,7,12-tris(methoxycarbonylmethyl)-4,5-dihydrotripyrrin-1,10(15H,17H)-dithione
CAS No.:207982-27-2
Molecular Formula:C₆₃H₇₀N₄O₂₀S₂
Molecular Weight:1267.4
Hs Code.:

14-Benzyloxycarbonyl-4-[5-benzyloxycarbonyl-4-(2-methoxycarbonylethyl)-3-(methoxycarbonylmethyl)pyrrol-2-ylmethyl]-2,8,13-tris(2-methoxycarbonylethyl)-3,7,12-tris(methoxycarbonylmethyl)-4,5-dihydrotripyrrin-1,10(15H,17H)-dithione

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Chemical Property of 14-Benzyloxycarbonyl-4-[5-benzyloxycarbonyl-4-(2-methoxycarbonylethyl)-3-(methoxycarbonylmethyl)pyrrol-2-ylmethyl]-2,8,13-tris(2-methoxycarbonylethyl)-3,7,12-tris(methoxycarbonylmethyl)-4,5-dihydrotripyrrin-1,10(15H,17H)-dithione

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Technology Process of 14-Benzyloxycarbonyl-4-[5-benzyloxycarbonyl-4-(2-methoxycarbonylethyl)-3-(methoxycarbonylmethyl)pyrrol-2-ylmethyl]-2,8,13-tris(2-methoxycarbonylethyl)-3,7,12-tris(methoxycarbonylmethyl)-4,5-dihydrotripyrrin-1,10(15H,17H)-dithione

There total 8 articles about 14-Benzyloxycarbonyl-4-[5-benzyloxycarbonyl-4-(2-methoxycarbonylethyl)-3-(methoxycarbonylmethyl)pyrrol-2-ylmethyl]-2,8,13-tris(2-methoxycarbonylethyl)-3,7,12-tris(methoxycarbonylmethyl)-4,5-dihydrotripyrrin-1,10(15H,17H)-dithione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 207982-26-1
14-Benzyloxycarbonyl-4-[5-benzyloxycarbonyl-4-(2-methoxycarbonylethyl)-3-(methoxycarbonylmethyl)pyrrol-2-ylmethyl]-2,8,13-tris(2-methoxycarbonylethyl)-3,7,12-tris(methoxycarbonylmethyl)-4,5-dihydrotripyrrin-1,10(15H,17H)-dione

: 207982-27-2
14-Benzyloxycarbonyl-4-[5-benzyloxycarbonyl-4-(2-methoxycarbonylethyl)-3-(methoxycarbonylmethyl)pyrrol-2-ylmethyl]-2,8,13-tris(2-methoxycarbonylethyl)-3,7,12-tris(methoxycarbonylmethyl)-4,5-dihydrotripyrrin-1,10(15H,17H)-dithione

Guidance literature:: With 2,4-bis(methylthio)-1,3-dithia-2,4-diphosphetane-2,4-disulfide; In 1,2-dimethoxyethane; for 0.166667h; Ambient temperature;
DOI:10.1039/a708134k

Reference yield: 30.0%

: 207982-26-1
14-Benzyloxycarbonyl-4-[5-benzyloxycarbonyl-4-(2-methoxycarbonylethyl)-3-(methoxycarbonylmethyl)pyrrol-2-ylmethyl]-2,8,13-tris(2-methoxycarbonylethyl)-3,7,12-tris(methoxycarbonylmethyl)-4,5-dihydrotripyrrin-1,10(15H,17H)-dione

: C₆₃H₇₀N₄O₂₁S

: 207982-27-2
14-Benzyloxycarbonyl-4-[5-benzyloxycarbonyl-4-(2-methoxycarbonylethyl)-3-(methoxycarbonylmethyl)pyrrol-2-ylmethyl]-2,8,13-tris(2-methoxycarbonylethyl)-3,7,12-tris(methoxycarbonylmethyl)-4,5-dihydrotripyrrin-1,10(15H,17H)-dithione

Guidance literature:: With 2,4-bis(methylthio)-1,3-dithia-2,4-diphosphetane-2,4-disulfide; In 1,2-dimethoxyethane; Ambient temperature;
DOI:10.1039/a708134k

Reference yield:

: 50622-64-5
benzyl 3-(2-methoxycarbonylethyl)-4-methoxycarbonylmethyl-5-methylpyrrole-2-carboxylate

: 207982-27-2
14-Benzyloxycarbonyl-4-[5-benzyloxycarbonyl-4-(2-methoxycarbonylethyl)-3-(methoxycarbonylmethyl)pyrrol-2-ylmethyl]-2,8,13-tris(2-methoxycarbonylethyl)-3,7,12-tris(methoxycarbonylmethyl)-4,5-dihydrotripyrrin-1,10(15H,17H)-dithione

Guidance literature:: Multi-step reaction with 7 steps

1: t-BuOCl / tetrahydrofuran / 3 h / Ambient temperature

2: tetrahydrofuran / 0.25 h

3: 1.) POCl₃ / 1.) 60 deg C, 30 min, 2.) 1,2-dichloroethene, 70 deg C, 4 h

4: t-BuOCl / tetrahydrofuran; diethyl ether / 0.33 h / 0 °C

5: AcONa / 1 h / 60 °C

6: 1.) SnCl₄, 2.) glacial AcOH / 1.) C₆H₆, r.t., 45 min, 2.) r.t., 1 h

7: 30 percent / 2,4-bis-methylsulfanyl-<1,3,2,4>dithiadiphosphetane disulfide / 1,2-dimethoxy-ethane / Ambient temperature

With tert-butylhypochlorite; sodium acetate; tin(IV) chloride; 2,4-bis(methylthio)-1,3-dithia-2,4-diphosphetane-2,4-disulfide; acetic acid; trichlorophosphate; In tetrahydrofuran; 1,2-dimethoxyethane; diethyl ether;
DOI:10.1039/a708134k