tetraphenylphosphonium pentathiacyclothioarsenate(III)

Base Information

Chemical Name:tetraphenylphosphonium pentathiacyclothioarsenate(III)
CAS No.:141948-86-9
Molecular Formula:AsS₆*C₂₄H₂₀P
Molecular Weight:606.714
Hs Code.:

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Chemical Property of tetraphenylphosphonium pentathiacyclothioarsenate(III)

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Technology Process of tetraphenylphosphonium pentathiacyclothioarsenate(III)

There total 1 articles about tetraphenylphosphonium pentathiacyclothioarsenate(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: sodium tetrasulfide

: 99021-99-5
tetraphenylphosphonium pentachlorothioarsenate(III)

: 141948-86-9
tetraphenylphosphonium pentathiacyclothioarsenate(III)

Guidance literature:: In acetonitrile; byproducts: NaCl, Na3AsS3, S8; dropwise addn. of a suspension of Na2S4 in CH3CN to a suspension of (P(C6H5)4)(As2SCl5) in CH3CN at 20°C with stirring; stirring for 15 h at 20°C; performed in the absence of moisture;; filtration; crystn. from filtrate at 5°C within several days; dried in vac.; elem. anal.;;

Reference yield: 55.0%

: sodium tetrasulfide

: 141948-86-9
tetraphenylphosphonium pentathiacyclothioarsenate(III)

: tetraphenylphosphonium heptasulfide

Guidance literature:: In acetonitrile; dropwise addn. of a Na2S4-suspension in CH3CN to (P(C6H5)4)(SAsS5) in CH3CN at 20°C with stirring; stirring at 20°C for 24 h; performed in the absence of moisture;; elem. anal.;;