dibromobis(diethyldithiocarbamato)((2,6-dimethylphenyl)imido)molybdenum(VI)

Base Information

• Chemical Name: dibromobis(diethyldithiocarbamato)((2,6-dimethylphenyl)imido)molybdenum(VI)
• CAS No.: 478158-42-8
• Molecular Formula: C₁₈H₂₉Br₂MoN₃S₄
• Molecular Weight: 671.46
• Mol file: 478158-42-8.mol

Synonyms:

Chemical Property of dibromobis(diethyldithiocarbamato)((2,6-dimethylphenyl)imido)molybdenum(VI)

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of dibromobis(diethyldithiocarbamato)((2,6-dimethylphenyl)imido)molybdenum(VI)

There total 1 articles about dibromobis(diethyldithiocarbamato)((2,6-dimethylphenyl)imido)molybdenum(VI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

MoO(Br)2(diethyldithiocarbamate)2 (95042-41-4,53548-92-8) + 2,6-dimethylaniline (87-62-7) → dibromobis(diethyldithiocarbamato)((2,6-dimethylphenyl)imido)molybdenum(VI) (478158-42-8)

Guidance literature:

With butyllithium; In tetrahydrofuran; under Ar atm. to soln. MoOBr2(dtc)2 in THF ligand and butyllithium were added and refluxed for 4 h; react. mixt. was filtered and evapd. to dryness, residue was dissolved in CH2Cl2 and layered with hexane, ppt. was filtered and dried in vacuo; elem. anal.;

DOI:10.1021/ic025642x

upstream raw materials:

MoO(Br)2(diethyldithiocarbamate)2

2,6-dimethylaniline

Refernces