C₁₈H₂₆F₂N₂O₂

Base Information

Chemical Name:C₁₈H₂₆F₂N₂O₂
CAS No.:1292321-49-3
Molecular Formula:C₁₈H₂₆F₂N₂O₂
Molecular Weight:340.413
Hs Code.:

C<sub>18</sub>H<sub>26</sub>F<sub>2</sub>N<sub>2</sub>O<sub>2</sub>

Synonyms:

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Chemical Property of C₁₈H₂₆F₂N₂O₂

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Technology Process of C₁₈H₂₆F₂N₂O₂

There total 10 articles about C₁₈H₂₆F₂N₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₄H₂₀Cl₃NO₅

: 1292321-49-3
C₁₈H₂₆F₂N₂O₂

Guidance literature:: Multi-step reaction with 8 steps

1: n-butyllithium / tetrahydrofuran / -78 °C

2: sodium hexamethyldisilazane / tetrahydrofuran / -78 °C

3: hydrogenchloride / methanol / 20 °C

4: triethylamine / dichloromethane / 20 °C

5: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran; water / 20 °C

6: diphenyl phosphoryl azide; N-ethyl-N,N-diisopropylamine / toluene / 100 °C

7: chloro-trimethyl-silane / dichloromethane / 20 °C

8: palladium 10% on activated carbon; hydrogen / ethanol

With hydrogenchloride; n-butyllithium; chloro-trimethyl-silane; diphenyl phosphoryl azide; palladium 10% on activated carbon; hydrogen; dihydrogen peroxide; sodium hexamethyldisilazane; triethylamine; N-ethyl-N,N-diisopropylamine; lithium hydroxide; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; toluene; 6: Curtius rearrangement;
DOI:10.1016/j.bmcl.2010.12.060

Reference yield:

: 1292321-47-1
C₂₉H₃₄F₂N₂O₅

: 1292321-49-3
C₁₈H₂₆F₂N₂O₂

Guidance literature:: Multi-step reaction with 6 steps

1: hydrogenchloride / methanol / 20 °C

2: triethylamine / dichloromethane / 20 °C

3: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran; water / 20 °C

4: diphenyl phosphoryl azide; N-ethyl-N,N-diisopropylamine / toluene / 100 °C

5: chloro-trimethyl-silane / dichloromethane / 20 °C

6: palladium 10% on activated carbon; hydrogen / ethanol

With hydrogenchloride; chloro-trimethyl-silane; diphenyl phosphoryl azide; palladium 10% on activated carbon; hydrogen; dihydrogen peroxide; triethylamine; N-ethyl-N,N-diisopropylamine; lithium hydroxide; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; toluene; 4: Curtius rearrangement;
DOI:10.1016/j.bmcl.2010.12.060

Reference yield:

: C₂₄H₂₆F₂N₂O₃

: 1292321-49-3
C₁₈H₂₆F₂N₂O₂

Guidance literature:: Multi-step reaction with 5 steps

1: triethylamine / dichloromethane / 20 °C

2: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran; water / 20 °C

3: diphenyl phosphoryl azide; N-ethyl-N,N-diisopropylamine / toluene / 100 °C

4: chloro-trimethyl-silane / dichloromethane / 20 °C

5: palladium 10% on activated carbon; hydrogen / ethanol

With chloro-trimethyl-silane; diphenyl phosphoryl azide; palladium 10% on activated carbon; hydrogen; dihydrogen peroxide; triethylamine; N-ethyl-N,N-diisopropylamine; lithium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; water; toluene; 3: Curtius rearrangement;
DOI:10.1016/j.bmcl.2010.12.060