mer-Λ-tris(1-phenylpyrazolato,N,C(2)')iridium(III)

Base Information

Chemical Name:mer-Λ-tris(1-phenylpyrazolato,N,C(2)')iridium(III)
CAS No.:562824-20-8
Molecular Formula:C₂₇H₂₁IrN₆
Molecular Weight:621.724
Hs Code.:

Synonyms:

Suppliers and Price of mer-Λ-tris(1-phenylpyrazolato,N,C(2)')iridium(III)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of mer-Λ-tris(1-phenylpyrazolato,N,C(2)')iridium(III)

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of mer-Λ-tris(1-phenylpyrazolato,N,C(2)')iridium(III)

There total 8 articles about mer-Λ-tris(1-phenylpyrazolato,N,C(2)')iridium(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1126-00-7
1-phenylpyrazole

: 562824-23-1,562824-20-8,359014-72-5
tris(1-phenyl-κC1-pyrazolato-κN2)iridium

Guidance literature:: In water; ethylene glycol; at 180 ℃; for 17h; Inert atmosphere;

Reference yield: 25.0%

: 1126-00-7
1-phenylpyrazole

: iridium(III) trisacetylacetonate

: 562824-23-1,562824-20-8,359014-72-5
tris(1-phenyl-κC1-pyrazolato-κN2)iridium

Guidance literature:: In glycerol; under N2 or Ar atm. using Schlenk techniques; amt. of 1-phenylpyrazole dissolved in glycerol; mixt. heated at reflux under N2 for 10 h; cooled; 1 M HCl added; ppt. collected by filtration; dissolved in hot CH2Cl2; vol. reduced; concd. soln. was flash-chromd. on silica gel (CH2Cl2 as eluent); soln. concd.; recrystd. (CH2Cl2/MeOH); elem. anal.;
DOI:10.1246/bcsj.77.751

Reference yield:

: 359014-72-5,562824-20-8,562824-23-1
mer-Λ-tris(1-phenylpyrazolato,N,C(2)')iridium(III)

: 359014-72-5,562824-20-8,562824-23-1
fac-Λ-tris(1-phenylpyrazolato,N,C(2)')iridium(III)

Guidance literature:: In acetonitrile; Irradiation (UV/VIS); soln. of Ir complex in CH3CN irradiated at 25°C; not isolated, detecteed by UV and CD spectra;
DOI:10.1002/ejic.200801254