(1S,2R)-epoxy-7'-phenylindane

Base Information

Chemical Name:(1S,2R)-epoxy-7'-phenylindane
CAS No.:1354558-51-2
Molecular Formula:C₁₅H₁₂O
Molecular Weight:208.26
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,2R)-epoxy-7'-phenylindane

Chemical Property:

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Technology Process of (1S,2R)-epoxy-7'-phenylindane

There total 6 articles about (1S,2R)-epoxy-7'-phenylindane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 324534-56-7
4-phenyl-1H-indene

: 1354558-51-2
(1S,2R)-epoxy-7'-phenylindane

Guidance literature:: 4-phenyl-1H-indene; With C₃₈H₄₂ClMnN₂O₄; 4-methylmorpholine N-oxide; In dichloromethane; at -78 ℃; for 0.25h;

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at -78 ℃;
DOI:10.1039/c1ob06780j

Reference yield:

: 7-phenyl-2,3-dihydro-1H-inden-1-one

: 1354558-51-2
(1S,2R)-epoxy-7'-phenylindane

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium tetrahydroborate / methanol / 1 h / 0 - 20 °C

2.1: Amberlyst 15 / hexane / 3 h / 0 - 20 °C / Reflux

3.1: C₃₈H₄₂ClMnN₂O₄; 4-methylmorpholine N-oxide / dichloromethane / 0.25 h / -78 °C

3.2: -78 °C

With sodium tetrahydroborate; C₃₈H₄₂ClMnN₂O₄; 4-methylmorpholine N-oxide; In methanol; hexane; dichloromethane;
DOI:10.1039/c1ob06780j

Reference yield:

: 6968-35-0
7-hydroxy-indan-1-one

: 1354558-51-2
(1S,2R)-epoxy-7'-phenylindane

Guidance literature:: Multi-step reaction with 5 steps

1.1: triethylamine / dichloromethane / 24 h / 20 °C

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / tetrahydrofuran; water / Inert atmosphere; Reflux

3.1: sodium tetrahydroborate / methanol / 1 h / 0 - 20 °C

4.1: Amberlyst 15 / hexane / 3 h / 0 - 20 °C / Reflux

5.1: C₃₈H₄₂ClMnN₂O₄; 4-methylmorpholine N-oxide / dichloromethane / 0.25 h / -78 °C

5.2: -78 °C

With sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; C₃₈H₄₂ClMnN₂O₄; sodium carbonate; 4-methylmorpholine N-oxide; triethylamine; In tetrahydrofuran; methanol; hexane; dichloromethane; water;
DOI:10.1039/c1ob06780j