HC(CC(CH₃)C(C₂H₅)C(CH₃)N)2BF(C₆F₅)

Base Information

Chemical Name:HC(CC(CH₃)C(C₂H₅)C(CH₃)N)2BF(C₆F₅)
CAS No.:1183675-97-9
Molecular Formula:C₂₃H₂₃BF₆N₂
Molecular Weight:452.25
Hs Code.:

HC(CC(CH<sub>3</sub>)C(C<sub>2</sub>H<sub>5</sub>)C(CH<sub>3</sub>)N)2BF(C<sub>6</sub>F<sub>5</sub>)

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Suppliers and Price of HC(CC(CH₃)C(C₂H₅)C(CH₃)N)2BF(C₆F₅)

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Chemical Property of HC(CC(CH₃)C(C₂H₅)C(CH₃)N)2BF(C₆F₅)

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Technology Process of HC(CC(CH₃)C(C₂H₅)C(CH₃)N)2BF(C₆F₅)

There total 1 articles about HC(CC(CH₃)C(C₂H₅)C(CH₃)N)2BF(C₆F₅) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 830-49-9
difluoro (pentafluorophenyl)borane

: 7375-42-0,151464-97-0
2,4,8,10-tetramethyl-3,9-diethyldipyrrolyl-5,7-methene hydrobromide

: 1183675-97-9
HC(CC(CH₃)C(C₂H₅)C(CH₃)N)2BF(C₆F₅)

Guidance literature:: With Et₃N; In dichloromethane; (Ar); glovebox; mixt. of bromide and Et3N (2 equiv.) in CH2Cl2 was stirred at room temp. for 15 min; soln. of B compd. in CH2Cl2 was added dropwise with stirring; reacted for 15 min; evapd. (vac.); chromd. (silica, hexane/toluene, 3/2); elem. anal.;
DOI:10.1021/om900402e

Reference yield: 86.0%

: (CH₃)3Si⁽¹⁺⁾*N(SO₂CF₃)2^(1-)=[(CH₃)3Si]N(SO₂CF₃)2

: 1183675-97-9
HC(CC(CH₃)C(C₂H₅)C(CH₃)N)2BF(C₆F₅)

: 1183676-08-5
(HC(CC(CH₃)C(C₂H₅)C(CH₃)N)2B(C₆F₅))2F⁽¹⁺⁾*N(SO₂CF₃)2^(1-)=[(HC(CC(CH₃)C(C₂H₅)C(CH₃)N)2B(C₆F₅))2F]N(SO₂CF₃)2

Guidance literature:: In dichloromethane; (Ar); glovebox; soln. of Me3SiN(SO2CF3)2 (0.5 equiv.) in CH2Cl2 was added dropwise with stirring to soln. of B compd. in CH2Cl2; stirred for 15 min; evapd. (vac.); recrystd. (CH2Cl2/hexane);
DOI:10.1021/om900402e

Reference yield:

: (CH₃)3Si⁽¹⁺⁾*N(SO₂CF₃)2^(1-)=[(CH₃)3Si]N(SO₂CF₃)2

: 1183675-97-9
HC(CC(CH₃)C(C₂H₅)C(CH₃)N)2BF(C₆F₅)

: 1183676-04-1
HC(CC(CH₃)C(C₂H₅)C(CH₃)N)2B(C₆F₅)⁽¹⁺⁾*N(SO₂CF₃)2^(1-)=[HC(CC(CH₃)C(C₂H₅)C(CH₃)N)2B(C₆F₅)]N(SO₂CF₃)2

Guidance literature:: In dichloromethane-d2; byproducts: (CH3)3SiF; (Ar); glovebox; soln. of Me3SiN(SO2CF3)2 (1 equiv.) in CD2Cl2 was added to B compd. in NMR tube; NMR monitoring;
DOI:10.1021/om900402e