(1S,2R)-2-(4-chlorophenyl)cyclohexanol

Base Information

Chemical Name:(1S,2R)-2-(4-chlorophenyl)cyclohexanol
CAS No.:1129273-72-8
Molecular Formula:C₁₂H₁₅ClO
Molecular Weight:210.704
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,2R)-2-(4-chlorophenyl)cyclohexanol

Chemical Property:

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Technology Process of (1S,2R)-2-(4-chlorophenyl)cyclohexanol

There total 2 articles about (1S,2R)-2-(4-chlorophenyl)cyclohexanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7150-18-7
3β-acetoxyetienic acid

: (+/-)-trans-2-(4-chlorophenyl)cyclohexanol

: 1129273-72-8
(1S,2R)-2-(4-chlorophenyl)cyclohexanol

: 91767-30-5
cis-2-(4-Chlor-phenyl)-cyclohexanol

: 3β-acetoxy-5-etienic acid (1S,2R)-2-naphthyl ester

: 3β-acetoxy-5-etienic acid (1S,2R)-2-naphthyl ester

Guidance literature:: With dmap; In dichloromethane; at 20 ℃; for 24h;
DOI:10.1080/00397911.2011.636498

Reference yield:

: 1129273-72-8
(1S,2R)-2-(4-chlorophenyl)cyclohexanol

: 91767-30-5
cis-2-(4-Chlor-phenyl)-cyclohexanol

Guidance literature:: With palladium(II) trifluoroacetate; hydrogen; toluene-4-sulfonic acid; (R)-segphos; In 2,2,2-trifluoroethanol; at 30 ℃; for 24h; under 5171.62 Torr; Overall yield = 92 percent; Overall yield = 59 mg; Optical yield = 83 percent ee; Glovebox;

Reference yield: 22.0%

: 1129273-72-8
(1S,2R)-2-(4-chlorophenyl)cyclohexanol

: cis-2-(4-chlorophenyl)cyclohexylamine

Guidance literature:: (1S,2R)-2-(4-chlorophenyl)cyclohexanol; With phthalimide; di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 0 - 25 ℃; Inert atmosphere;

With hydrazine hydrate; In ethanol; for 2h; Inert atmosphere; Reflux;
DOI:10.1002/chem.201604440