Technology Process of Benzene, (1-methoxy-1,6-nonadienyl)-, (E,Z)-
There total 4 articles about Benzene, (1-methoxy-1,6-nonadienyl)-, (E,Z)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
trimethylsilyl trifluoromethanesulfonate; N-ethyl-N,N-diisopropylamine;
In
dichloromethane;
for 22h;
Yield given;
Ambient temperature;
DOI:10.1021/jo00034a038
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 99 percent / montmorrillonite K10 clay / pentane / 16 h
2: TMSOTf, i-Pr2NEt / CH2Cl2 / 22 h / Ambient temperature
With
trimethylsilyl trifluoromethanesulfonate; montmorrillonite K10 clay; N-ethyl-N,N-diisopropylamine;
In
dichloromethane; pentane;
DOI:10.1021/jo00034a038
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 70 percent / Jones reagent / acetone / 1.5 h / 25 °C
2: 99 percent / montmorrillonite K10 clay / pentane / 16 h
3: TMSOTf, i-Pr2NEt / CH2Cl2 / 22 h / Ambient temperature
With
jones reagent; trimethylsilyl trifluoromethanesulfonate; montmorrillonite K10 clay; N-ethyl-N,N-diisopropylamine;
In
dichloromethane; acetone; pentane;
DOI:10.1021/jo00034a038