δ--δ.δ-dimethyl-α-carbethoxy-valeriansaeure-ethylester

Base Information

• Chemical Name: δ--δ.δ-dimethyl-α-carbethoxy-valeriansaeure-ethylester
• CAS No.: 19355-36-3
• Molecular Formula: C₁₉H₂₈O₄
• Molecular Weight: 320.429

Synonyms:

Chemical Property of δ--δ.δ-dimethyl-α-carbethoxy-valeriansaeure-ethylester

Chemical Property:

Purity/Quality:

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Technology Process of δ--δ.δ-dimethyl-α-carbethoxy-valeriansaeure-ethylester

There total 1 articles about δ--δ.δ-dimethyl-α-carbethoxy-valeriansaeure-ethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

sodium diethylmalonate (996-82-7) + 3-Methyl-3-m-tolyl-butan-1-ol → δ--δ.δ-dimethyl-α-carbethoxy-valeriansaeure-ethylester (19355-36-3)

Guidance literature:

Multistep reaction; (i) TsCl, Py, (ii) /BRN= 6900104/, THF;

DOI:10.1016/S0040-4020(01)92590-6

Reference yield:

δ--δ.δ-dimethyl-α-carbethoxy-valeriansaeure-ethylester (19355-36-3) → <2,4-Dinitrophenyl>-(+/-)-ar-himachalen-yl-sulfid

Guidance literature:

Multi-step reaction with 4 steps

1: HCl, AcOH

2: polyphosphoric acid / petroleum ether

3: (i) benzene, (ii) H₂, PtO₂, AcOH

4: AlCl₃ / CH₂Cl₂

With hydrogenchloride; aluminium trichloride; PPA; acetic acid; In dichloromethane; Petroleum ether;

DOI:10.1016/S0040-4020(01)92590-6

Reference yield:

δ--δ.δ-dimethyl-α-carbethoxy-valeriansaeure-ethylester (19355-36-3) → δ--δ,δ-dimethyl-valeriansaeure (19355-37-4)

Guidance literature:

With hydrogenchloride; acetic acid;

DOI:10.1016/S0040-4020(01)92590-6

upstream raw materials:

sodium diethylmalonate

Downstream raw materials:

δ--δ,δ-dimethyl-valeriansaeure

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