C₂₂H₃₉BO₃Si

Base Information

Chemical Name:C₂₂H₃₉BO₃Si
CAS No.:1438826-28-8
Molecular Formula:C₂₂H₃₉BO₃Si
Molecular Weight:390.446
Hs Code.:

C<sub>22</sub>H<sub>39</sub>BO<sub>3</sub>Si

Synonyms:

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Chemical Property of C₂₂H₃₉BO₃Si

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Technology Process of C₂₂H₃₉BO₃Si

There total 4 articles about C₂₂H₃₉BO₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 16692-57-2
1-bromo-2-(pent-1-en-1-yl)benzene

: 1438826-28-8
C₂₂H₃₉BO₃Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: toluene-4-sulfonic acid hydrazide; sodium acetate trihydrate / tetrahydrofuran / 12 h / 80 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere

2.2: 24 h / -78 - 20 °C / Inert atmosphere; Glovebox

3.1: (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 3,4,7,8-Tetramethyl-o-phenanthrolin / tetrahydrofuran / 24 h / 80 °C / Inert atmosphere; Glovebox

4.1: C₂₀H₂₈Cl₂Rh₂ / 1 h / 0 °C

With n-butyllithium; (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 3,4,7,8-Tetramethyl-o-phenanthrolin; C₂₀H₂₈Cl₂Rh₂; sodium acetate trihydrate; toluene-4-sulfonic acid hydrazide; In tetrahydrofuran; hexane;
DOI:10.1021/ja403462b

Reference yield:

: 13397-96-1
1-bromo-2-pentylbenzene

: 1438826-28-8
C₂₂H₃₉BO₃Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere

1.2: 24 h / -78 - 20 °C / Inert atmosphere; Glovebox

2.1: (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 3,4,7,8-Tetramethyl-o-phenanthrolin / tetrahydrofuran / 24 h / 80 °C / Inert atmosphere; Glovebox

3.1: C₂₀H₂₈Cl₂Rh₂ / 1 h / 0 °C

With n-butyllithium; (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 3,4,7,8-Tetramethyl-o-phenanthrolin; C₂₀H₂₈Cl₂Rh₂; In tetrahydrofuran; hexane;
DOI:10.1021/ja403462b

Reference yield:

: 1438824-72-6
2-pentylphenyl dimethylsilane

: 1438826-28-8
C₂₂H₃₉BO₃Si

Guidance literature:: Multi-step reaction with 2 steps

1: (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 3,4,7,8-Tetramethyl-o-phenanthrolin / tetrahydrofuran / 24 h / 80 °C / Inert atmosphere; Glovebox

2: C₂₀H₂₈Cl₂Rh₂ / 1 h / 0 °C

With (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 3,4,7,8-Tetramethyl-o-phenanthrolin; C₂₀H₂₈Cl₂Rh₂; In tetrahydrofuran;
DOI:10.1021/ja403462b