C₂₅H₃₅N₃O₅S

Base Information

Chemical Name:C₂₅H₃₅N₃O₅S
CAS No.:1423117-90-1
Molecular Formula:C₂₅H₃₅N₃O₅S
Molecular Weight:489.636
Hs Code.:

C<sub>25</sub>H<sub>35</sub>N<sub>3</sub>O<sub>5</sub>S

Synonyms:

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Chemical Property of C₂₅H₃₅N₃O₅S

Chemical Property:

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Technology Process of C₂₅H₃₅N₃O₅S

There total 15 articles about C₂₅H₃₅N₃O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1423040-35-0
methyl (2S,4R)-4-{[(2-{(1R,3R)-1-acetoxy-3-[(tert-butoxycarbonyl)amino]-4-methylpentyl}-1,3-thiazol-4-yl)carbonyl]amino}-2-methyl-5-phenylpentanoate

: 1423117-90-1
C₂₅H₃₅N₃O₅S

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; at 0 ℃; for 2h;
DOI:10.1002/cjoc.201200984

Reference yield:

: 5-benzyl-3-methylenepyrrolidin-2-one

: 1423117-90-1
C₂₅H₃₅N₃O₅S

Guidance literature:: Multi-step reaction with 8 steps

1.1: triethylamine; dmap / dichloromethane / 24 h / 20 °C

2.1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 24 h / 20 °C / 760.05 Torr

3.1: lithium hydroxide; water / tetrahydrofuran / 3 h / 20 °C

4.1: diethyl ether / 20 °C

5.1: trifluoroacetic acid / dichloromethane / 4 h / 20 °C / Cooling with ice

6.1: triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; 1-hydroxy-7-aza-benzotriazole / N,N-dimethyl-formamide / 0.08 h

6.2: 24 h / 0 - 20 °C

7.1: pyridine / 12 h

8.1: hydrogenchloride / 1,4-dioxane / 2 h / 0 °C

With pyridine; hydrogenchloride; dmap; 1-hydroxy-7-aza-benzotriazole; palladium 10% on activated carbon; water; hydrogen; triethylamine; trifluoroacetic acid; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; lithium hydroxide; In tetrahydrofuran; 1,4-dioxane; diethyl ether; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1002/cjoc.201200984

Reference yield:

: 852202-38-1
(R)-tert-butyl (2-methylhex-5-en-3-yl)carbamate

: 1423117-90-1
C₂₅H₃₅N₃O₅S

Guidance literature:: Multi-step reaction with 7 steps

1.1: osmium(VIII) oxide; 4-methyl-morpholine / water; acetone / 34 h / 20 - 40 °C

2.1: sodium periodate / tetrahydrofuran; water / 0 - 20 °C

3.1: boron trifluoride diethyl etherate / tetrahydrofuran / 0.17 h / -78 °C

3.2: 2.5 h / -78 - 20 °C

4.1: sodium hydroxide; water / tetrahydrofuran / 24 h / 20 °C

5.1: triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; 1-hydroxy-7-aza-benzotriazole / N,N-dimethyl-formamide / 0.08 h

5.2: 24 h / 0 - 20 °C

6.1: pyridine / 12 h

7.1: hydrogenchloride / 1,4-dioxane / 2 h / 0 °C

With 4-methyl-morpholine; pyridine; hydrogenchloride; sodium periodate; osmium(VIII) oxide; 1-hydroxy-7-aza-benzotriazole; boron trifluoride diethyl etherate; water; triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; water; N,N-dimethyl-formamide; acetone;
DOI:10.1002/cjoc.201200984