1-(trans-4-methyl-5-ethylcyclopentenyl)dimethylcarbinol

Base Information

Chemical Name:1-(trans-4-methyl-5-ethylcyclopentenyl)dimethylcarbinol
CAS No.:96689-51-9
Molecular Formula:C₁₁H₂₀O
Molecular Weight:168.279
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(trans-4-methyl-5-ethylcyclopentenyl)dimethylcarbinol

Chemical Property:

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Technology Process of 1-(trans-4-methyl-5-ethylcyclopentenyl)dimethylcarbinol

There total 8 articles about 1-(trans-4-methyl-5-ethylcyclopentenyl)dimethylcarbinol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5682-72-4
2-ethyl-3-methylcyclopent-2-en-1-one

: 96689-51-9
1-(trans-4-methyl-5-ethylcyclopentenyl)dimethylcarbinol

Guidance literature:: Multi-step reaction with 4 steps

1: 5percent rhodium on carbon, sodium carbonate, hydrogen / petroleum ether / 12 h

2: 56 percent / hydrazine hydrate, triethylamine / ethanol / 12 h / Heating

3: 1.) TMG, I₂, 2.) guanidine base / 1.) ether, RT, 30 min, 2.) 80-90 deg C, 2 h

4: 1.) Li / 1.) ether, 15 h, 2.) -60 deg C, 30 min

With rhodium contaminated with carbon; hydrogen; iodine; lithium; sodium carbonate; hydrazine hydrate; guanidine nitrate; triethylamine; N,N,N',N'-tetramethylguanidine; In ethanol; Petroleum ether;
DOI:10.1021/jo00214a008

Reference yield:

: 76047-58-0
(2S,3S)-2-Ethyl-3-methyl-cyclopentanone

: 96689-51-9
1-(trans-4-methyl-5-ethylcyclopentenyl)dimethylcarbinol

Guidance literature:: Multi-step reaction with 3 steps

1: 56 percent / hydrazine hydrate, triethylamine / ethanol / 12 h / Heating

2: 1.) TMG, I₂, 2.) guanidine base / 1.) ether, RT, 30 min, 2.) 80-90 deg C, 2 h

3: 1.) Li / 1.) ether, 15 h, 2.) -60 deg C, 30 min

With iodine; lithium; hydrazine hydrate; guanidine nitrate; triethylamine; N,N,N',N'-tetramethylguanidine; In ethanol;
DOI:10.1021/jo00214a008

Reference yield:

: 76047-57-9
(2S,3R)-2-Ethyl-3-methyl-cyclopentanone

: 96689-51-9
1-(trans-4-methyl-5-ethylcyclopentenyl)dimethylcarbinol

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / hydrazine hydrate, triethylamine / ethanol / 12 h / Heating

2: 1.) TMG, I₂, 2.) guanidine base / 1.) ether, RT, 30 min, 2.) 80-90 deg C, 2 h

3: 1.) Li / 1.) ether, 15 h, 2.) -60 deg C, 30 min

With iodine; lithium; hydrazine hydrate; guanidine nitrate; triethylamine; N,N,N',N'-tetramethylguanidine; In ethanol;
DOI:10.1021/jo00214a008