1-Hydroxy-7-methoxymitosene methylcarbonate

Base Information

• Chemical Name: 1-Hydroxy-7-methoxymitosene methylcarbonate
• CAS No.: 78776-08-6
• Molecular Formula: C₁₇H₁₈N₂O₈
• Molecular Weight: 378.339
• Mol file: 78776-08-6.mol

Synonyms:

Chemical Property of 1-Hydroxy-7-methoxymitosene methylcarbonate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-Hydroxy-7-methoxymitosene methylcarbonate

There total 2 articles about 1-Hydroxy-7-methoxymitosene methylcarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.7%

1-hydroxy-7-methoxymitosene (40863-79-4) + methyl chloroformate (79-22-1) → 1-Hydroxy-7-methoxymitosene methylcarbonate (78776-08-6)

Guidance literature:

With pyridine; In dichloromethane; for 24h; Ambient temperature;

DOI:10.1021/jm00142a013

Reference yield:

1-Acetoxy-7-methoxymitosene (40863-78-3) → 1-Hydroxy-7-methoxymitosene methylcarbonate (78776-08-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 77.7 percent / 30percent ammonium hydroxide / methanol / 10 h / Ambient temperature

2: 45.7 percent / pyridine / CH₂Cl₂ / 24 h / Ambient temperature

With pyridine; ammonium hydroxide; In methanol; dichloromethane;

DOI:10.1021/jm00142a013

upstream raw materials:

1-hydroxy-7-methoxymitosene

methyl chloroformate

1-Acetoxy-7-methoxymitosene