C₃₁H₄₂N₂O₂*ClH

Base Information

Chemical Name:C₃₁H₄₂N₂O₂*ClH
CAS No.:1561903-38-5
Molecular Formula:C₃₁H₄₂N₂O₂*ClH
Molecular Weight:511.148
Hs Code.:

C<sub>31</sub>H<sub>42</sub>N<sub>2</sub>O<sub>2</sub>*ClH

Synonyms:

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Chemical Property of C₃₁H₄₂N₂O₂*ClH

Chemical Property:

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Technology Process of C₃₁H₄₂N₂O₂*ClH

There total 6 articles about C₃₁H₄₂N₂O₂*ClH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3-(azacyclotridecan-1-yl)propanenitrile

: 1561903-38-5
C₃₁H₄₂N₂O₂*ClH

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium aluminium tetrahydride / diethyl ether / 0.25 h / 0 - 33 °C / Inert atmosphere

2.1: sodium iodide / tetrahydrofuran / 0.42 h / 20 °C / Inert atmosphere

2.2: 1 h / 20 °C

3.1: methanol / 0.5 h

3.2: 16 h / 45 °C

4.1: hydrogenchloride / methanol; diethyl ether; chloroform; pentane

With hydrogenchloride; lithium aluminium tetrahydride; sodium iodide; In tetrahydrofuran; methanol; diethyl ether; chloroform; pentane;
DOI:10.1039/c3ob42309c

Reference yield:

: 295-03-4
azacyclotridecane

: 1561903-38-5
C₃₁H₄₂N₂O₂*ClH

Guidance literature:: Multi-step reaction with 5 steps

1.1: triethylamine / N,N-dimethyl-formamide / 16 h / 70 °C / Inert atmosphere

2.1: lithium aluminium tetrahydride / diethyl ether / 0.25 h / 0 - 33 °C / Inert atmosphere

3.1: sodium iodide / tetrahydrofuran / 0.42 h / 20 °C / Inert atmosphere

3.2: 1 h / 20 °C

4.1: methanol / 0.5 h

4.2: 16 h / 45 °C

5.1: hydrogenchloride / methanol; diethyl ether; chloroform; pentane

With hydrogenchloride; lithium aluminium tetrahydride; triethylamine; sodium iodide; In tetrahydrofuran; methanol; diethyl ether; chloroform; N,N-dimethyl-formamide; pentane;
DOI:10.1039/c3ob42309c

Reference yield:

: 947-04-6,25038-74-8
2-azacyclotridecanone

: 1561903-38-5
C₃₁H₄₂N₂O₂*ClH

Guidance literature:: Multi-step reaction with 6 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 16 h / 20 °C / Inert atmosphere; Reflux

2.1: triethylamine / N,N-dimethyl-formamide / 16 h / 70 °C / Inert atmosphere

3.1: lithium aluminium tetrahydride / diethyl ether / 0.25 h / 0 - 33 °C / Inert atmosphere

4.1: sodium iodide / tetrahydrofuran / 0.42 h / 20 °C / Inert atmosphere

4.2: 1 h / 20 °C

5.1: methanol / 0.5 h

5.2: 16 h / 45 °C

6.1: hydrogenchloride / methanol; diethyl ether; chloroform; pentane

With hydrogenchloride; lithium aluminium tetrahydride; triethylamine; sodium iodide; In tetrahydrofuran; methanol; diethyl ether; chloroform; N,N-dimethyl-formamide; pentane;
DOI:10.1039/c3ob42309c